Abstract. The technological flowchart of purification of medium-and low-activity waste from Co-60 and Cs-137 is developed and introduced. The developed purification scheme has been successfully tested using genuine medium-and low-level liquid radioactive waste of radiochemical production containing complexing and colloid forming components (complexons, surfactants). The optimal conditions of the presented method of purification ensure reduction of the residual specific activity of 60Co and 137Cs radionuclides in the solution to less than 0,9 Bq per litre.