“…Because this substance and its derivatives are applied in such a variety of different fields and has been recognized as a carcinogenic and hepatotoxic agent, their quantitative determination is of great analytical importance, attracting the interest of many researchers. Different methods for the determination of hydrazine and its compounds, such as flow injection analysis with fluorimetric (Ensafi and Rezaei 1998) and chemiluminescence (Song, Wang, and Zhao 2001;Safavi and Baezzat 1998;Lv, Huang, and Zhang 2001) detection, potentiometric (Mo et al 2000;George, Nagaraja, and Balasubramanian 2007), spectrophotometric (Hasan 1988;Ortega-Barrales et al 1997;Ensafi and Naderi 1997;Afkhami and Assl 2001), and capillary electrophoresis (Siangproh et al 2005) methods have been described in literature. Electroanalytical techniques seem to provide direct and efficient methods for the detection of hydrazine and its derivatives.…”