is study investigates the effect of liquid gallium (Ga) on metal foils made of titanium (Ti), niobium (Nb), and molybdenum (Mo). e Ti, Nb, and Mo foils were heated in liquid Ga at 120 ∘ C for a maximum of two weeks. Aer heating, the changes in the morphology and the chemical composition of the metal foils were analyzed by using a �eld emission scanning electron microscope, energy-dispersive X-ray spectrometer, X-ray diffractometer, and X-ray photoelectron spectrometer. e results of the analysis indicated that the Nb foil showed the minimum adhesion of liquid Ga to the surface while the maximum amount of liquid Ga was observed to adhere to the Ti foil. In addition, the Nb foil was oxidized and the Mo foil was reduced during the heating process. Considering these effects, we conclude that Mo may be used as an alternative encapsulation material for Ga in addition to Nb, which is used as the conventional encapsulation material, due to its chemical resistance against oxidation in hot liquid Ga.