1981
DOI: 10.1016/s0021-9673(00)81957-3
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Resolution of linear gramicidins by preparative reversed-phase high-performance liquid chromatography

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Cited by 52 publications
(34 citation statements)
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“…Methods previously described in the literature (43)(44)(45) The 1 H NMR spectra were obtained with a Varian VXRwere used to obtain gramicidin A from the commercially 500S spectrometer ( Palo Alto, California ) . The first increavailable gramicidin D (Sigma Chemical Co., St. Louis, ment of the nuclear Overhauser effect spectroscopy Missouri).…”
Section: Methodsmentioning
confidence: 99%
“…Methods previously described in the literature (43)(44)(45) The 1 H NMR spectra were obtained with a Varian VXRwere used to obtain gramicidin A from the commercially 500S spectrometer ( Palo Alto, California ) . The first increavailable gramicidin D (Sigma Chemical Co., St. Louis, ment of the nuclear Overhauser effect spectroscopy Missouri).…”
Section: Methodsmentioning
confidence: 99%
“…Though this method was an improvement on the existing LC methods described in literature for gramicidin [6,8,11,12], some minor gramicidin components were still not resolved.…”
Section: Optimization Of Chromatographic Methodsmentioning
confidence: 99%
“…In an effort to further improve the analysis method for gramicidin we examined the procedures described in literature [6,8]. Isocratic systems containing methanol-0.005M ammonium sulphate (74:26) [8] or methanol-water (75:25) [6] were evaluated.…”
Section: Optimization Of Chromatographic Methodsmentioning
confidence: 99%
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