Retention behaviour of some coumarins in normal-phase high-performance thin-layer and column chromatography

Bieganowska, M. L.; Głowniak, Kazimierz

doi:10.1007/bf02259026

Cited by 20 publications

(5 citation statements)

References 28 publications

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“…Nowadays several efficient analytical methods (e.g HPLC, HPTLC, high speed countercurrent chromatography) for the selective separation, detection and quantification of 7-isopentenyloxycoumarin in plant extracts are also available [30,39,[44][45][46][47][48].…”

Section: Natural and Synthetic Sourcesmentioning

confidence: 99%

Insights on Novel Biologically Active Natural Products: 7-Isopentenyloxycoumarin

Epifano

Pelucchini

Curini

et al. 2009

Natural Product Communications

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7-Isopentenyloxycoumarin is a prenyloxyphenylpropanoid derivative found in low concentration in a restricted number of plant families (Apiaceae, Asteraceae, and Rutaceae). Synthetic schemes were recently developed enabling sufficient quantities of the title coumarin to be obtained in order to evidence its valuable biological effects, mainly as an anti-cancer agent. The aim of this review is to examine the phytochemical and pharmacological properties of this compound.

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Section: Natural and Synthetic Sourcesmentioning

confidence: 99%

Insights on Novel Biologically Active Natural Products: 7-Isopentenyloxycoumarin

Epifano

Pelucchini

Curini

et al. 2009

Natural Product Communications

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“…Bergapten is phototoxic – , mutagenic , , and tumorigenic . For these reasons, different methodologies have been proposed for also determining bergapten contents in biological fluids ,– . Recently , , bergapten has been reported to be the component responsible for serious problems caused in humans by regular consumption of Earl Grey tea, an alimentary preparation containing bergamot extracts.…”

Section: Introductionmentioning

confidence: 99%

Comparison of the Volatile Constituents in Cold-Pressed Bergamot Oil and a Volatile Oil Isolated by Vacuum Distillation

Belsito

Carbone

Gioia

et al. 2007

J. Agric. Food Chem.

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The vacuum distillation of bergamot peels furnishes a high-quality essential oil that is totally bergapten-free. This oil was compared with that produced by distillation of cold-pressed oils and those commercially available. The oil obtained by vacuum distillation of the bergamot vegetable matrix shows a composition quite similar to that of the cold-pressed oil. It also displays qualitative characteristics that are superior with respect to those normally observed for essential oils isolated by distillation of cold-pressed oils. Oils isolated by the method presented here can constitute ideal candidates in producing foods, for example, Earl Grey tea, and cosmetic preparations.

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“…palustre contain coumarins such as isoimperatorin, (+)oxypeucedanin, ostruthol, (+)-oxypeucedanin hydrate, columbianadin (4), peulustrin (5), and as a minor component apterin (6). It has also been reported that the extracts of fruits, herb, and roots contain a similar set of coumarins: mainly isoimperatorin, imperatorin, columbianadin, oxypeucedanin, and oxypeucedanin hydrate (7,8). Preliminary extraction tests suggested that the active compounds were in the non-polar fraction obtained from the root material of P. palustre (9).…”

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confidence: 96%

Isobyakangelicin Angelate; A Novel Furanocoumarin fromPeucedanum palustre

Vuorela¹,

Erdelmeier²,

Nyiredy³

et al. 1988

Planta Med

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Isobyakangelicin angelate, a new furanocoumarin and the five known coumarins, columbianadin, (+)-oxypeucedanin, (±)-oxypeucedanin hydrate, ostruthol, and isoimperatorin, were isolated from roots of Peucedanum palustre (L.) Moench using medium-pressure liquid chromatography [MPLC] with normal phase and subsequently with reversed phase as stationary phases. The mobile phases were optimized in TLC and HPLC preassays according to the "PRISMA" system and then transferred without modification to preparative MPLC separations. The structures of the compounds were elucidated by a combination of spectroscopic methods, among others the rotating frame Overhauser enhancement spectroscopy [ROESY] experiment.

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Retention behaviour of some coumarins in normal-phase high-performance thin-layer and column chromatography

Cited by 20 publications

References 28 publications

Insights on Novel Biologically Active Natural Products: 7-Isopentenyloxycoumarin

Insights on Novel Biologically Active Natural Products: 7-Isopentenyloxycoumarin

Comparison of the Volatile Constituents in Cold-Pressed Bergamot Oil and a Volatile Oil Isolated by Vacuum Distillation

Isobyakangelicin Angelate; A Novel Furanocoumarin fromPeucedanum palustre

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