Review headspace‐gas chromatographic analysis of medicinal and aromatic plants and flowers

Bicchi, Carlo; Joulain, Daniel

doi:10.1002/ffj.2730050302

Cited by 57 publications

(27 citation statements)

References 85 publications

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“…5.1) is becoming a powerful technique not only for the analysis of fruit samples (Dirinck et al 1984;Ibanez et al 1999), and food samples such as olive oil (Rapparini and Rotondi 2002), but is also widely employed in ecological and environmental studies (Bicchi and Joulain 1990;Charron et al 1996, Ruther andHilker 1998;Jacobsen 1997;Takeoka and Full 1997;Hewitt 1998;Baraldi et al 1999;Butrym and Hartman 1999;Mendes et al 2000;Rapparini et al 2000a;Rapparini et al 2001), investigations on tissue cultures physiology (Predieri et al 1999;Rapparini et al 2000b), in forensic science (Goldbaum et al 1964;Pohl and Keller 1985), and in perfume research (Bedoukian et al 1979 Rapparini) nique has been reviewed elsewhere (Schaefer 1981;Jacobsen 1997). The headspace sampling system ( Fig.…”

Section: B Isolation and Concentration Of Pear Volatilesmentioning

confidence: 99%

Pear Fruit Volatiles

Rapparini

Predieri

2002

Horticultural Reviews

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Section: B Isolation and Concentration Of Pear Volatilesmentioning

confidence: 99%

Pear Fruit Volatiles

Rapparini

Predieri

2002

Horticultural Reviews

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“…Solidphase microextraction (SPME) technique can solve many of the above problems (Lee et al, 1998). Solidphase microextraction (SPME) is an advanced technique to be coupled to GC/MS or HPLC for identification of pollutants (Benfenati et al, 1999;Pawliszyn, 1997;Baser et al, 2003;Yıldırım et al, 2004;Joulain, 1985;Mookherjee et al, 1998;Mookherjee et al, 1989;Bicchi and Joulain, 1990;Brunke et al, 1993;Kaiser, 1993;Brunke et al, 1992 andKolb andEttre, 1997). SPME was performed with a commercially available polydimethylsiloxane/divinylbenzene (PDMS/DVB) fiber with a film thickness of 65 μm (Supelco).…”

Section: Spme Analysesmentioning

confidence: 97%

Characterization of an urban landfill soil by using physicochemical analysis and solid phase microextraction (SPME)—GC/MS

Banar

Özkan

Vardar³

2006

Environ Monit Assess

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We have aimed at characterizing top soil samples taken in-situ from five different locations of the unregulated dumping site in Eskişehir/Turkey for a period of six months. The study is the first attempt in the city and in Turkey, regarding particularly the SPME (Solid Phase Microextraction Technique) analysis method utilized. A comprehensive research has been conducted to produce critical soil data to be used for indicating current risks as well as the urgency of rehabilitating the site and establishing a sanitary landfill in the site. Conventional physicochemical analytical methods and SPME technique were used to analyze the samples. Physicochemical analyses were performed for determining the pH, total dried matter, volatile matter, total nitrogen, phosphorus, macro elements and heavy metals. Meteorological data were also recorded for the same period. SPSS.10.0 statistical program was used to determine the correlation between meteorological data and physicochemical analysis results. Mean values were used in the correlation analyses. These data indicated that the air temperature and precipitation have significant effects on soil characteristics. SPME, coupled with GC/MS, was used to identify eighty six volatile and semi-volatile organic compounds contained in soil samples. The samples were extracted by headspace SPME with heating (DeltaHS-SPME). SPME analyses were conducted using a commercially available polydimethylsiloxane/divinylbenzene (PDMS/DVB) fiber having a film thickness of 65 microm (Supelco) as a capture medium. The experimentally optimized headspace sampling conditions were arranged (15 min. at 50 degrees C) before a 30 min. sampling period.

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“…There is no need to remove the fiber during the entire operation. The same fiber can be used over and over again if handled properly (Pawliszyn, 1997;Baser et al, 2003;Yıldırım et al, 2004;Joulain, 1985;Mookherjee et al, 1998;Mookherjee et al, 1989;Bicchi and Joulain, 1990;Brunke et al, 1993;Kaiser, 1993;Brunke et al, 1992;Kolb and Ettre, 1997).…”

Section: Spme Analysis Of Leachatesmentioning

confidence: 97%

Characterization of the Leachate in an Urban Landfill by Physicochemical Analysis and Solid Phase Microextraction-GC/MS

Banar

Özkan

Kürkçüoğlu

2006

Environ Monit Assess

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The aim of this study is to evaluate extensively the characterization and identification of major pollutant parameters by paying attention to the organic chemical pollution for unregulated dumping site leachate in Eskişehir/Turkey. The study that is first and only one research has been very important data related with before new sanitary landfill site in Eskişehir city. For this purpose, in this study leachate samples were collected in-situ at monthly interval for a period of 8 months. Firstly, thirty three physicochemical parameters were monitored. Secondly, SPME technique was used for identification of organic pollutants. Meteorological data were also recorded for the same sampling period to correlate meteorological data and physicochemical parameters. Mean values are used in the correlation analysis. Correlation is shown only for the relationship between air temperature and NO(3) (-). No correlation has been found between rain and leachate quality parameters since the amount of rain was very low during the sampling period. However, analysis results were generally decreased in winter season when each parameter and each sampling point are examined separately. According to correlation between every parameter, especially solid content and dissolved oxygen concentration of leachate is affecting to other parameters. Also, sodium and potassium are changing proportionally with same parameters (suspended solids, fixed solids, dissolved oxygen) and high correlation between chloride and heavy metal concentration is showing. The results were statistically evaluated by use of SPSS 10.0 program. Second part of the study, the leachate was extracted by Solid Phase Microextraction (SPME) technique and then analyzed. Of the methodologies tested in this study, the best one selected was based on 100 micro m polydimethylsiloxane coated fiber (PDMS), headspace with heating (Delta HS) sampling mode and an extraction time of 15 min. at a temperature of 50 degrees C. Thirty three organic compounds in leachate were identified by GC/MS.

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Review headspace‐gas chromatographic analysis of medicinal and aromatic plants and flowers

Cited by 57 publications

References 85 publications

Pear Fruit Volatiles

Pear Fruit Volatiles

Characterization of an urban landfill soil by using physicochemical analysis and solid phase microextraction (SPME)—GC/MS

Characterization of the Leachate in an Urban Landfill by Physicochemical Analysis and Solid Phase Microextraction-GC/MS

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