Abstract:In this work the spark plasma sintering (SPS) technique has been explored as an alternative consolidation route for producing ultra-fine grained Fe-14Cr model alloys containing a dispersion of oxide nanoparti-cles. Elemental powders of Fe and Cr, and nanosized Y 2 O 3 powder have been mechanically alloyed in a planetary ball mill and rapidly sintered in a spark plasma furnace. Two alloys, with nominal compositions Fe-14%Cr and Fe-14% Cr-0.3%Y 2 O 3 (wt.%), have been fabricated and their microstructure and mechanical properties investigated. The results have been compared with those obtained for other powder metal-lurgy processed alloys of the same composition but consolidated by hot isostatic pressing. The SPS tech-nique under the present conditions has produced Fe-14Cr materials that apparently exhibit different microstructures yielding inferior mechanical properties than the counterpart material consolidated by hot isostatic pressing. Although the presence of a dispersion of Y-rich particles is evident, the oxide dis-persion strengthened (ODS) Fe-14Cr alloy consolidated by SPS exhibits poor tensile properties. The extensive decoration of the powder particle surfaces with Cr-rich precipitates and the residual porosity appear to be responsible for the impaired properties of this ODS alloy consolidated by SPS.