2022
DOI: 10.1021/acs.langmuir.2c00438
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Robust and Transparent Antifogging Polysilsesquioxane Film Containing a Hydroxy Group

Abstract: Poly­(glycidyloxypropyl)­silsesquioxane (PGPS) was successfully synthesized by hydrolysis and polycondensation using the nitrogen flow method. A poly­(3-(2,3-dihydroxypropoxypropyl)­silsesquioxane) (PSQ-OH) film was prepared via two routes. In route A, PSQ-OH was prepared by the hydrolysis of the epoxy group of PGPS in an aqueous hydrochloric acid (HCl)/tetrahydrofuran solution, affording a diol group; then, PSQ-OH was coated on a glass substrate and heated. The antifogging performance of the PSQ-OH film was e… Show more

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Cited by 9 publications
(28 citation statements)
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“…Water was purified using a Millipore Mill-Q UV system. The glass substrates were washed using an alkaline solution according to our previous study . A Kapton film (thickness, 12.5 μm) was purchased from AZ One Corporation (Osaka, Japan).…”
Section: Methodsmentioning
confidence: 99%
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“…Water was purified using a Millipore Mill-Q UV system. The glass substrates were washed using an alkaline solution according to our previous study . A Kapton film (thickness, 12.5 μm) was purchased from AZ One Corporation (Osaka, Japan).…”
Section: Methodsmentioning
confidence: 99%
“…PSQ-Diol/EG films were prepared according to a reported procedure . First, a 50 wt % PSQ-Gly/EG–THF solution was coated onto a cleaned glass substrate using an applicator (clearance gap of 50 μm) and heated at 80 and 150 °C for 1 and 0.5 h, respectively.…”
Section: Methodsmentioning
confidence: 99%
See 3 more Smart Citations