This research examines the simultaneous retrieval of surface soil moisture and salt concentrations using hyperspectral reflectance data in an arid environment. We conducted laboratory and outdoor field experiments in which we examined three key soil variables: soil moisture, salt and texture (silty loam, clay and silty clay). The soil moisture content models for multiple textures (M_SMC models) were based on selected hyperspectral reflectance data located around 1460, 1900 and 2010 nm and resulted in R 2 values higher than 0.933. Meanwhile, the soil salt concentrations were also accurately (R 2 > 0.748) modeled (M_SSC models) based on wavebands located at 540, 1740, 2010 and 2350 nm. When the different texture samples were mixed (SL + C + SC models), soil moisture was still accurately retrieved (R 2 = 0.937) but the soil salt not as well (R 2 = 0.47). After stratifying the samples by retrieved soil moisture levels, the R 2 of calibrated M_SSC SMC models for soil salt concentrations improved to 0.951. This two-step method also showed applicability for analyzing soil-salt samples in the field. The M_SSC SMC models resulted in R 2 values equal to 0.912 when moisture is lower than 0.15, and R 2 values equal to 0.481 when soil moisture is between 0.15 and 0.2.