Sample Preparation for Trace Analysis
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The article contains sections titled: 1 Subject and Scope 2 Working Fields 3 Contamination and Decontamination 4 Quantitation of Trace‐Analytical Measurements and Their Quality Assurance 4.1 Basic Considerations 4.2 Uncertainty Concept 4.3 Calibration 4.4 Validation 4.5 Limit of Decision, Detection, and Determination 4.6 Analytical Quality Assurance 5 Sampling, Sample Preservation, and Sample Preparation 5.1 Sampling and Sample Preservation 5.2 Sample Preparation 5.2.1 General Aspects 5.2.2 Sample Preparation for Inorganic Trace Analysis 5.2.3 Sample Preparation for Organic Trace Analysis 6 Inorganic Trace Analysis 6.1 Introduction 6.2 Spectroscopic Methods 6.2.1 Atomic Absorption Spectroscopy (AAS) 6.2.2 Inductively Coupled Plasma Optical Emission Spectroscopy (ICP‐OES) 6.2.3 Inductively Coupled Plasma Mass Spectroscopy (ICP‐MS) 6.2.4 Comparison of AAS, ICP‐OES, and ICP‐MS 6.2.5 X‐ray Fluorescence Spectroscopy (XRF) 6.3 Electrochemical Analytical Methods 6.3.1 Potentiometry–Ion‐selective Electrodes (ISE) 6.3.2 Voltammetry/Polarography 6.3.3 Comparison of Electrochemical Analytical Methods 6.4 Neutron Activation Analysis (NAA) 7 Organic Trace Analysis 7.1 Introduction 7.2 Gas Chromatography (GC) 7.3 High Performance Liquid Chromatography (HPLC) 8 Other Techniques for Trace Analysis 8.1 Methods of Classical Chemical Analysis 8.2 Methods of the Determination of Group and Sum Parameters 8.3 Enzyme and Immunochemical Analysis 9 Examples of Trace Analysis 9.1 Analysis of Fresh Water for Trace Elements by ICP‐MS 9.2 Determination of Pt in Soil Samples by GFAAS 9.3 Determination of Polyaromatic Hydrocarbons by GC/MS 9.4 Analysis of Explosives by HPLC/UV 10 Perspective References
The article contains sections titled: 1 Subject and Scope 2 Working Fields 3 Contamination and Decontamination 4 Quantitation of Trace‐Analytical Measurements and Their Quality Assurance 4.1 Basic Considerations 4.2 Uncertainty Concept 4.3 Calibration 4.4 Validation 4.5 Limit of Decision, Detection, and Determination 4.6 Analytical Quality Assurance 5 Sampling, Sample Preservation, and Sample Preparation 5.1 Sampling and Sample Preservation 5.2 Sample Preparation 5.2.1 General Aspects 5.2.2 Sample Preparation for Inorganic Trace Analysis 5.2.3 Sample Preparation for Organic Trace Analysis 6 Inorganic Trace Analysis 6.1 Introduction 6.2 Spectroscopic Methods 6.2.1 Atomic Absorption Spectroscopy (AAS) 6.2.2 Inductively Coupled Plasma Optical Emission Spectroscopy (ICP‐OES) 6.2.3 Inductively Coupled Plasma Mass Spectroscopy (ICP‐MS) 6.2.4 Comparison of AAS, ICP‐OES, and ICP‐MS 6.2.5 X‐ray Fluorescence Spectroscopy (XRF) 6.3 Electrochemical Analytical Methods 6.3.1 Potentiometry–Ion‐selective Electrodes (ISE) 6.3.2 Voltammetry/Polarography 6.3.3 Comparison of Electrochemical Analytical Methods 6.4 Neutron Activation Analysis (NAA) 7 Organic Trace Analysis 7.1 Introduction 7.2 Gas Chromatography (GC) 7.3 High Performance Liquid Chromatography (HPLC) 8 Other Techniques for Trace Analysis 8.1 Methods of Classical Chemical Analysis 8.2 Methods of the Determination of Group and Sum Parameters 8.3 Enzyme and Immunochemical Analysis 9 Examples of Trace Analysis 9.1 Analysis of Fresh Water for Trace Elements by ICP‐MS 9.2 Determination of Pt in Soil Samples by GFAAS 9.3 Determination of Polyaromatic Hydrocarbons by GC/MS 9.4 Analysis of Explosives by HPLC/UV 10 Perspective References
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