2016
DOI: 10.1039/c6ra03736d
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l-Leucine supported on superparamagnetic silica-encapsulated γ-Fe2O3nanoparticles: design, characterization, and application as a green catalyst for highly efficient synthesis of thiazoloquinolines

Abstract: A new superparamagnetic silica-encapsulated γ-Fe2O3 supported l-leucine was successfully prepared and characterized by XRD, SEM, EDS, VSM, TGA, and FT-IR analysis. It catalyzed the synthesis of thiazoloquinolines derivatives.

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Cited by 22 publications
(6 citation statements)
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“…γ-Fe 2 O 3 /SiO 2 composite particles were prepared in analogy with previously reported work from our group. 33 The coprecipitation method was used to prepare γ-Fe 2 O 3 , 34,35 dissolving 0.401 g of FeCl 2 •4H 2 O and 1.092 g of FeCl 3 •6H 2 O in 2 and 4 mL of a 2 M HCl solution, respectively. Both iron precursor solutions were stirred (800 rpm).…”
Section: ■ Experimental Sectionmentioning
confidence: 99%
“…γ-Fe 2 O 3 /SiO 2 composite particles were prepared in analogy with previously reported work from our group. 33 The coprecipitation method was used to prepare γ-Fe 2 O 3 , 34,35 dissolving 0.401 g of FeCl 2 •4H 2 O and 1.092 g of FeCl 3 •6H 2 O in 2 and 4 mL of a 2 M HCl solution, respectively. Both iron precursor solutions were stirred (800 rpm).…”
Section: ■ Experimental Sectionmentioning
confidence: 99%
“…[62] The method was successfully employed in the synthesis of sixteen various derivatives of the specific ring fusion and the yields were good. Finally, for thiazolo [3,2-a]quinolone, the one-pot four component solventfree synthesis using L-leucine as the catalyst was the most promising method, [67] as it was applied to a wide variety of substrates and was high yielding.…”
Section: Discussionmentioning
confidence: 99%
“…These improvements have been made in order to increase the accessible sites/zones on the surface of catalyst, greater catalyst reactivity and selectivity, thermal stability and nally easy separation. Fe 3 O 4 , 12,13 NiFe 2 O 4 , [14][15][16] CoFe 2 O 4 , 17 CuFe 2 O 4 , [18][19][20] MnFe 2 O 4 , 21 Ni-Cu-ZnFe 2 O 4 , 22 BiFeO 3 , 23 FeAl 2 O 4 24 and ZnCrFeO 4 25 as a core, and metals, [26][27][28] silica, [29][30][31][32] polymers, [33][34][35] carbon nanotubes and sheets, [36][37][38][39][40] cellulose, 41 small organic molecules, 42,43 ionic liquids, 44,45 and organosulfonic acids 46,47 have been used as a coating.…”
Section: Introductionmentioning
confidence: 99%