1959
DOI: 10.1021/ac60154a025
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Sealed Tube Combustions for Determination of Carbon- 14 and Total Carbon

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Cited by 105 publications
(30 citation statements)
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“…Samples for δ 13 C POM and δ 13 C PHY measurements were acidified with dilute hydrochloric acid and oven-dried overnight at 60°C just prior to carbon isotope determination. Particulate organic matter was converted into CO 2 using the high-temperature (850°C, 5 h) sealed-quartz tube combustion method with copper oxide as oxidant (Buchanan and Corcoran, 1959) as the low-temperature (550°C, 1 h) combustion method can lead to large analytical uncertainty (Tao et al, 2001).…”
Section: Methodsmentioning
confidence: 99%
“…Samples for δ 13 C POM and δ 13 C PHY measurements were acidified with dilute hydrochloric acid and oven-dried overnight at 60°C just prior to carbon isotope determination. Particulate organic matter was converted into CO 2 using the high-temperature (850°C, 5 h) sealed-quartz tube combustion method with copper oxide as oxidant (Buchanan and Corcoran, 1959) as the low-temperature (550°C, 1 h) combustion method can lead to large analytical uncertainty (Tao et al, 2001).…”
Section: Methodsmentioning
confidence: 99%
“…The average precision of this method for %OC and atomic C : N was + 1.5% of the measured value for plant tissues and fine-grained sediments and * 3% for the more heterogeneous coarse-grained sediments. Stable carbon isotope compositions were determined by the sealed-tube combustion method (Buchanan and Corcoran 1959) and are reported as parts per thousand relative variation (6) from the PDB standard (Craig 1953). The average precision of this measurement was 20. lo/o0 for plant tissues and fine sediments and +0.2a/oo for coarse sediments.…”
Section: Methodsmentioning
confidence: 99%
“…The envelope was placed in a quartz ampule, which was evacuated and flame sealed, based on modifications to the procedure described by Buchanan & Corcoran (1959). Ampules were combusted at 900°C for 3 h and allowed to cool.…”
Section: Methodsmentioning
confidence: 99%