2015
DOI: 10.3998/ark.5550190.p009.169
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Selective acetylation of primary amino groups with phenyl acetate; simple synthesis of N,N´-diacetyl polyamines

Abstract: Phenyl acetate was studied as a general reagent for highly selective N-acetylation of primary amino groups in the presence of alcohol and secondary amino groups. Two polyamines, namely 1,8-diamino-4-azaoctane (Spd) and 1,12-diamino-4,9-diazadodecane (Spm), were N,N´-diacetylated with an efficient and mild methodology.

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