“…All spectral data match those previously reported. 27 Synthesis of 2-Hydroxypyridine (14). Following the general procedure, the crude product was purified using silica gel column chromatography (DCM−MeOH = 20:1) to produce the desired product 14; 14 was isolated as a brown solid (100 mg, 88% yield); 1 H NMR (400 MHz, DMSO-d) δ 11.59 (s, 1H), 7.46−7.32 (m, 2H), 6.31 (d, J = 9.2 Hz, 1H), 6.15 (td, J = 6.5, 0.8 Hz, 1H).…”