Various mechanical behaviors of ultrafine-grained (UFG) materials produced by equal channel angular pressing (ECAP) generally exhibit distinctive characteristics from those of conventional grained materials, so that the relevant studies have received sustained attention in recent years. [1][2][3][4][5][6][7][8][9][10][11][12][13][14][15][16] Apparently, the understanding of the fatigue properties (among various mechanical properties) of such UFG materials is of particular importance for their practical engineering applications, many investigators have thus been attempting to explore the fatigue deformation mechanisms of UFG materials, especially of UFG copper, with different emphases. [17][18][19][20][21][22][23][24][25][26][27][28][29][30][31][32][33][34] It is now commonly recognized that the low-cycle fatigue damage in UFG materials primarily results from the formation of shear bands (SBs), which can extend over far larger scales than the initial grain size, [18][19][20][21][22][23][24][25][26] and that the cyclic softening phenomenon as well as the deterioration in fatigue life under strain-amplitude-controlled tests in the low-cycle fatigue (LCF) regime is attributed to grain coarsening due to instabilities of the ECAPed structures during cycling. [21,22,27,32,33] On the contrary, the fatigue life of UFG materials obtained under stress-controlled tests in the highcycle fatigue (HCF) regime is normally enhanced greatly as compared to their conventional counterparts. [21,27] However, the details about cyclic deformation microstructures and shear band features in LCF and HCF regimes, respectively, are less understood so far. To further understand the possibly different fatigue deformation mechanisms of UFG copper in LCF and HCF regimes, the present contribution is to report the effect of the applied stress amplitude on the cyclic stress response behavior, surface damage features as well as relevant microstructural changes of such UFG copper materials. The applied stress amplitudes ranging from 100 MPa to 200 MPa are adopted to ensure that fatigue tests are carried out within both LCF and HCF regimes.
Experimental ProceduresThe rod of UFG copper (99.98 %) of 20 mm in diameter was produced by the ECAP process. Ten passages of extrusion were performed to introduce an equivalent shear strain of about 11.5. All pressings were carried out by rotating each sample about the longitudinal axis by 90°in the same direction between consecutive passes (i.e. so-called route Bc [3] ), using a die angle f = 90°. Fatigue specimens with a gauge section of 2 × 2 × 4 mm 3 were carefully spark-machined from the as-prepared rod. Before the fatigue tests, the specimens were electro-polished to produce a strain-free and mirror-like surface for microscopic observations. Stress-controlled (R = -1) fatigue tests were performed in vacuum at room temperature with a frequency of 5 Hz using a servo-hydraulic testing machine (Shimadzu SEM Servopulser). Three different applied stress amplitudes Dr/2 of 100 MPa, 150 MPa and 200 MPa were adopted....