Silylcarbonylation of 1,5-dienes accompanied by acyl radical cyclization

Ryu, Ilhyong; Nagahara, K.; Kurihara, Akio; Komatsu, Mitsuo; Sonoda, Noboru

doi:10.1016/s0022-328x(97)00167-8

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Cyclizations Of 5-hexenoyl Radicals2

Consecutive Radical Reactions1

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Cited by 14 publications

(3 citation statements)

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“…248 Here, the sequence is initiated by addition of a tris(trimethylsilyl)silyl radical to the least substituted terminus of the diene. Carbonylation and acyl radical cyclization then ensues in the normal way.…”

Section: Cyclizations Of 5-hexenoyl Radicalsmentioning

confidence: 99%

“…A further variant on the radical carbonylation/acyl radical cyclization theme involves the silyl carbonylation of hexa-1,5-dienes (Scheme 100). 248 Here, the sequence is initiated by addition of a tris(trimethylsilyl)silyl radical to the least substituted terminus of the diene. Carbonylation and acyl radical cyclization then ensues in the normal way.…”

Section: Cyclizations Of 5-hexenoyl Radicalsmentioning

confidence: 99%

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Chemistry of Acyl Radicals

et al. 1999

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Section: Cyclizations Of 5-hexenoyl Radicalsmentioning

confidence: 99%

Section: Cyclizations Of 5-hexenoyl Radicalsmentioning

confidence: 99%

Chemistry of Acyl Radicals

et al. 1999

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“…An unoptimized 51% yield was obtained 108 . The addition of (TMS) 3 SiH to substituted 1,5-dienes in the presence of CO has been studied by Ryu and coworkers 110 …”

Section: Consecutive Radical Reactionsmentioning

confidence: 99%