Simultaneous determination of cadmium and lead in wine by electrothermal atomic absorption spectrometry

Freschi, Gian Paulo Giovanni; Dakuzaku, Carolina Sinabucro; Moraes, Mercedes de; Nóbrega, Joaquim A.; Neto, José Anchieta Gomes

doi:10.1016/s0584-8547(01)00331-7

Cited by 61 publications

(45 citation statements)

References 22 publications

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“…Two Chardonnay wines, one from Tikveš region (Chardonnay-1) and the other from Skopje region (Chardonnay), presented similar contents of Cd (1.50 and 1.46 μg/L) which were not statistically different (p>0.05). The results are in a good agreement with those reported by Cvetković et al for Macedonian white wines (2006), similar to results for Slovenian wines (Kristl et al 2001), Brazilian wines (Freschi et al 2001) as well as Argentinean wines (Lara et al 2005). In addition, the mean value of Cd in this study (1.75 μg/L) was slightly lower compared to the results obtained for Spanish white wines (mean 3.44 μg/L) (Mena et al 1996).…”

Section: Elemental Characterization Of Winessupporting

confidence: 92%

“…The highest content of Pb was present in Smederevka-1 wine (28.5 μg/L) and Riesling-1 (24.7 μg/L), and lowest in Riesling-2 wine (2.01 μg/L). The results obtained are in a good agreement with those previously reported for Macedonian wines (Karadjova et al 2007) and Brazilian wines (Freschi et al 2001). In addition, Macedonian wines presented lower amounts of Pb (on average 16.9 μg/L) compared to data for Croatian wines reported by Tariba et al (2011) (on average 33 μg/L) and Banović et al (2009) (on average 197 μg/L), as well as lower compared to Serbian wines (Ražić et al 2007), Ethiopian white wines (Woldemariam and Chandravanshi 2011) and wines from the Korean market (Kim 2004).…”

Section: Elemental Characterization Of Winessupporting

confidence: 92%

“…In fact, flame atomic absorption is a very common technique for detecting metals and metalloids in different samples, including wine too (Freschi et al 2001;Stafilov and Karadjova 2009;Kinaree and Chanthai 2013). It is very reliable and simple to use.…”

Section: Flame Atomic Absorption Spectrometry and Etaas Methodsmentioning

confidence: 99%

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Determination of Pb and Cd in Macedonian Wines by Electrothermal Atomic Absorption Spectrometry (ETAAS)

et al. 2015

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In this study, electrothermal atomic absorption spectrometry (ETAAS) was used for determination of lead and cadmium in Macedonian white wines. Wine samples, without prior purification, were directly injected into the ETAAS system, using matrix modifiers for Pb and Cd. The standard addition method was used for quantitative analysis of Pb and Cd content. Reliability of the method was verified by determination of selected validation characteristics. The results of the measurements indicated satisfactory precision and accuracy, confirming that the method is accurate and convenient for quantitative analysis. The lead and cadmium concentrations were ranged between 2-28.5 and 0.4-5.69 μg/L, respectively. The levels were below the maximal allowed concentration in wine and compare well with those reported for similar wines from other parts of the world.

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Section: Elemental Characterization Of Winessupporting

confidence: 92%

Section: Elemental Characterization Of Winessupporting

confidence: 92%

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Determination of Pb and Cd in Macedonian Wines by Electrothermal Atomic Absorption Spectrometry (ETAAS)

et al. 2015

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“…Therefore, it has been necessary for analytical chemists to evaluate the environmental and healthy quantities based on accurate determination of Cd 2+ and Pb 2+ both in environmental and biological samples. For this purpose, the analytical methods including electrothermal atomic absorption spectrometry (ETAAS) [6][7][8][9][10][11][12][13], graphite furnace AAS [14][15][16], electroanalytical methods [17,18], inductively coupled plasmaatomic emission spectrometry (ICP-AES) [19] and inductively coupled plasma-mass spectrometry (ICP-MS) [20,21] are generally used. Most of these methods have disadvantages as far as cost and instruments used in routine analysis are concerned.…”

Section: Introductionmentioning

confidence: 99%

Simultaneous preconcentration of lead and cadmium ions with methyltrioctylammonium chloride supported on microcrystalline naphthalene and determination by flame atomic absorption spectrometry

2010

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A sensitive and selective preconcentration method has been developed for the determination of trace amounts of lead and cadmium ions by using naphthalenemethyltrioctylammonium chloride as an adsorbent. Lead and cadmium ions were retained by the adsorbent in the minicolumn as PbI4 2-and CdI4 2-, respectively. The column was washed by 5 mL of 2 mol L -1 nitric acid solution to elute the adsorbed cations. The collected eluents then were determined by flame atomic absorption spectrometry (FAAS). Potential factors affecting on the recovery of the analytes were investigated. Meanwhile optimum conditions were established. The preconcentration factor for lead (II) and cadmium (II) have been 300 and 100, respectively. The calibration curves were linear in the range of 3 to 100 ng mL -1 for Pb 2+ and in the range of 1 to 100 ng mL -1 for Cd 2+ , in the original water samples. The detection limits for Pb 2+ and Cd 2+ are 0.42 and 0.072 ng mL -1 respectively. On the other hand, the relative standard deviation (RSD) for 11 replicate measurements of 20 ng mL -1 Pb 2+ and Cd 2+ were 2.2% and 1.4% in the initial solution respectively (n=11). The developed method was successfully applied for the determination of trace Pb 2+ and Cd 2+ ions in a variety of water samples. Cadmium Lead FAAS Preconcentration Microcrystalline naphthalene

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“…Methods described so far include atomic absorption spectrometry (3,12,13), inductively coupled plasma optical emission spectrometry (14), inductively coupled plasma mass spectrometry (15,16), energy dispersive X-ray fl uorescence (17), potentiometric stripping analysis, and differential pulse anodic stripping voltammetry (13,18). The most common among them for determining Pb at trace levels is graphite furnace atomic absorption spectrometry (GFAAS) (14,(19)(20)(21)(22), a selective, simple, and highly sensitive method, adequate for direct determination in various matrices.…”

mentioning

confidence: 99%

Determination of Lead in Croatian Wines by Graphite Furnace Atomic Absorption Spectrometry

Tariba

Pizent²,

Kljaković-Gašpić³

2011

Archives of Industrial Hygiene and Toxicology

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A method has been developed for direct determination of lead in wine by graphite furnace atomic absorption spectrometry (GFAAS) with Zeeman-effect background correction. The thermal behaviour of Pb during pyrolysis and atomisation stages was investigated without matrix modifi er and in the presence of Pd(NO 3 ) 2 , Pd(NO 3 ) 2 + Mg(NO 3 ) 2 x 6H 2 O, and NH 4 H 2 PO 4 + Mg(NO 3 ) 2 x 6H 2 O as matrix modifi ers. A simple 1:1 dilution of wine samples with Pd(NO 3 ) 2 as a matrix modifi er proved optimal for accurate determination of Pb in wine. Mean recoveries were 106 % for red and 114 % for white wine, and the detection limit was 3 μg L -1 . Within-run precision of measurements for red and white wine was 2.1 % and 1.8 %, respectively. in home-made wines. There were no statistically signifi cant differences (P<0.05) in Pb concentration between commercial and home-made wines or between red and white wines.

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Simultaneous determination of cadmium and lead in wine by electrothermal atomic absorption spectrometry

Cited by 61 publications

References 22 publications

Determination of Pb and Cd in Macedonian Wines by Electrothermal Atomic Absorption Spectrometry (ETAAS)

Determination of Pb and Cd in Macedonian Wines by Electrothermal Atomic Absorption Spectrometry (ETAAS)

Simultaneous preconcentration of lead and cadmium ions with methyltrioctylammonium chloride supported on microcrystalline naphthalene and determination by flame atomic absorption spectrometry

Determination of Lead in Croatian Wines by Graphite Furnace Atomic Absorption Spectrometry

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