Single crystal growth of l-tartaric acid and its characterization for optical applications

Khan, Naghma; Shandilya, Kopal; Kumar, Ravinder; Krishna, A. G. Gopala; Chopra, Samridhi; Yadav, Sudha; Moona, Girija; Jewariya, Mukesh

doi:10.1007/s10854-020-02998-4

Cited by 10 publications

(4 citation statements)

References 19 publications

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“…Stretching of the CO bond of the carboxylic acids present in tartaric acid triggered the peaks in this IR band. 90,91 The presence of tartaric acid in the CuA-Tar metallogel was indicated by this finding. Similarly, the IR peaks at 732 cm −1 , 1076 cm −1 , 1125 cm −1 , 1322 cm −1 , 1434 cm −1 , and 1611 cm −1 show the presence of copper acetate.…”

Section: Resultsmentioning

confidence: 59%

“…94,95 A series of FTIR bands ranging from 900 cm À1 to 1000 cm À1 show the C-C stretching modes of vibration. 91 The band at 800 cm À1 , 822 cm À1 , and 876 cm À1 confirm the OH out of plane bending, COO wagging, and CH 2 rocking vibration modes within the material, respectively. The absorption bands at 642 cm À1 and 662 cm À1 are associated with the C-H out-of-plane bending mode and COO bending mode, respectively.…”

Section: Ft-ir Pxrd Raman and Tga Analysis Of Cua-tar Metallogelmentioning

confidence: 79%

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A multistimulus-responsive self-healable supramolecular copper(ii)-metallogel derived from l-(+) tartaric acid: an efficient Schottky barrier diode

et al. 2022

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Section: Resultsmentioning

confidence: 59%

Section: Ft-ir Pxrd Raman and Tga Analysis Of Cua-tar Metallogelmentioning

confidence: 79%

A multistimulus-responsive self-healable supramolecular copper(ii)-metallogel derived from l-(+) tartaric acid: an efficient Schottky barrier diode

et al. 2022

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“…The X‐ray powder diffraction (XRD) pattern of the MLTA powder, shown in Figure 1a, indicates the formation of a supramolecular structure, which exhibits a pattern unlike the mere superposition of melamine and L‐TA diffraction peaks; [35,36] only a few weakened peaks corresponding to residual melamine units remain at 2

{\theta }

≈17.66°, 26.16°, and 28.77° [37] . Fourier‐transform infrared spectroscopy (FTIR) measurements (Figure 1b) further confirm the formation of a supramolecular assembly of melamine and L‐TA.…”

Section: Resultsmentioning

confidence: 99%

Polymeric Carbon Nitride with Chirality Inherited from Supramolecular Assemblies

et al. 2023

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The facile synthesis of chiral materials is of paramount importance for various applications. Supramolecular preorganization of monomers for thermal polymerization has been proven as an effective tool to synthesize carbon and carbon nitride‐based (CN) materials with ordered morphology and controlled properties. However, the transfer of an intrinsic chemical property, such as chirality from supramolecular assemblies to the final material after thermal condensation, has never been shown. Here, we report the large‐scale synthesis of chiral CN materials capable of enantioselective recognition. To achieve this, we designed supramolecular assemblies with a chiral center that remains intact at elevated temperatures. The optimized chiral CN demonstrates an enantiomeric preference of ca. 14%; CN electrodes were also prepared and show stereoselective interactions with enantiomeric probes in electrochemical measurements. By adding chirality to the properties transferrable from monomers to the final product of a thermal polymerization, this study confirms the potential of using supramolecular precursors to produce carbon and CN materials and electrodes with designed chemical properties.

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“…The complex band with maxima at 1740 and 1720 cm -1 corresponds to the valence vibrations of the C=O bond of the unsubstituted carboxyl group [23]. These bands are absent in the spectra of carboxylic acid salts, but there are bands in the region of ~1550-1610 and ~1300-1400 cm -1 , respectively, related to asymmetric and symmetrical valence vibrations of ionized groups of COO - [24].…”

Section: Synthesis and Characterization Of Bismuth Tartratementioning

confidence: 98%

Thermal transformations of bismuth (III) tartrates

Afonina

Timakova

et al. 2022

Chim.Tech.Acta

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The processes of oxidative thermolysis of bismuth tartrates [Bi(NO3)(C4H4O6)]·3H2O and BiC4H3O6·H2O precipitated from bismuth nitrate solutions was studied by the methods of X-ray diffraction, thermal analysis, IR spectroscopy and chemical analysis. The staging of thermal transformation processes was determined. Morphological studies of initial precursors and the final products of their thermal transformations were carried out. The expediency of obtaining fine-crystal powders of the tetragonal bismuth oxide modification β-Bi2O3 with uniform sized particles by oxidative thermolysis of BiC4H3O6∙H2O was shown.

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Single crystal growth of l-tartaric acid and its characterization for optical applications

Cited by 10 publications

References 19 publications

A multistimulus-responsive self-healable supramolecular copper(ii)-metallogel derived from l-(+) tartaric acid: an efficient Schottky barrier diode

A multistimulus-responsive self-healable supramolecular copper(ii)-metallogel derived from l-(+) tartaric acid: an efficient Schottky barrier diode

Polymeric Carbon Nitride with Chirality Inherited from Supramolecular Assemblies

Thermal transformations of bismuth (III) tartrates

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