This appendix contains Scanning Electron Microscopy Images of large gibbsite particles found in the heel of Hanford Tank 241-S-112. These images show the morphology and large size of the gibbsite typically found in Hanford waste heels. These samples are known to be gibbsite because Al and O where the only EDS observable elements of significant concentration in the particles and because gibbsite was the dominant Al-O-bearing phase observed by XRD in the samples.