2016
DOI: 10.1016/j.cej.2015.07.029
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Single stage and countercurrent extraction of 5-hydroxymethylfurfural from aqueous phase systems

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Cited by 47 publications
(31 citation statements)
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“…Due to the efficient countercurrent extraction in the herein developed tubular reactor, over 99% of the produced 5-HMF is present in the organic phase (see Supporting Information). This is in good agreement to results reported by Sindermann et al 31 for countercurrent extraction of 5-HMF on a technical scale. We believe this is a major benefit of our concept with regard to an overall 5-HMF production process.…”
Section: Biphasic Countercurrent Reactorsupporting
confidence: 93%
“…Due to the efficient countercurrent extraction in the herein developed tubular reactor, over 99% of the produced 5-HMF is present in the organic phase (see Supporting Information). This is in good agreement to results reported by Sindermann et al 31 for countercurrent extraction of 5-HMF on a technical scale. We believe this is a major benefit of our concept with regard to an overall 5-HMF production process.…”
Section: Biphasic Countercurrent Reactorsupporting
confidence: 93%
“…primary and secondary alcohols, ketones), which has been widely studied and showed good performance in enhancing 5-HMF yield. [40][41][42][43] In the biphasic catalyzed system, the formed 5-HMF was continuously extracted from aqueous phase to organic solvent. So 5-HMF was isolated from water in a considerable extent and the rehydration side-reaction can hardly proceed.…”
Section: Introductionmentioning
confidence: 99%
“…The stirred-pulsed DN15 extraction column was especially developed for rapid and uncomplicated investigations of continuous countercurrent extraction on a laboratory scale, e.g., for process development. The column has already been successfully applied for various separation tasks, e.g., extractive separation of enantiomers [58] or methyl esters [59][60][61]. During these investigations, high separation efficiency was achieved in the column, resulting from miniaturization and from the agitatedpulsed operating mode.…”
Section: Extraction Columnmentioning
confidence: 99%