Sketchy synthesis of Mn3O4, Mn3O4/AC and Mn3O4/CNT composites for application of/in energy cache

Madhuri, Sakaray; Chakra, Chidurala Shilpa; Katlakunta, Sadhana; Divya, Velpula

doi:10.1016/j.matpr.2022.06.247

Cited by 4 publications

(4 citation statements)

References 17 publications

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“…The crystallite size, D , estimated using the above standard formula, was consistent with that assessed by Madhuri et al 49 and Ristić et al 50 (Table 1). Using Bragg's law, 2 d hkl sin θ = nλ , the interplanar spacing, d , between the atoms was calculated, where n is the order of diffraction ( n = 1).…”

Section: Resultssupporting

confidence: 87%

Biological synthesis of manganese oxide nanoparticles from aerial parts of Prunus dulcis and their in vitro investigation of medical properties

Aarthi,

Anitha

2023

Applied Organom Chemis

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The field of functional nanohybrid material is an emerging research area in material science due to its vast range of applications. The use of novel technology and innovative therapeutics has led to potent applications, including controlling the size of nanoparticles (NPs). This has resulted in a novel report on the synthesis of manganese oxide NPs using aerial parts of queen of roses Prunus dulcis (almond) leaves, seed, and seed oil (using Clevenger apparatus), which functions as a reducing agent. Manganese sulfate was used as a precursor in the synthesis process. The synthesized nanohybrid Mn3O4 NPs were studied using different characteristics techniques such as X‐ray diffraction (XRD), Fourier transform infrared spectroscopy (FTIR), scanning electron microscopy (SEM), and energy‐dispersive X‐ray spectroscopy (EDX). The photoluminescence spectra display the blue emission ranging from 483.2 to 486.5 nm. The biosynthesized Mn3O4 NPs were tested for bactericidal activity and showed tremendous inhibition against gram‐positive and gram‐negative bacteria. The antioxidant activity of Mn3O4 NPs was enhanced using 2,2‐diphenyl‐1‐picrylhydrazyl (DPPH) assay, which revealed the higher activity of Mn3O4 NPs from P. dulcis leaf extract. In vitro cytotoxicity of hybrid Mn3O4 NPs was examined using 3‐(4,5‐dimethylthiazol‐2‐yl)‐2,5‐diphenyltetrazolium bromide (MTT) assay against cervical cancer (HeLa cell line) with different concentrations. The results showed an IC50 value of 61.97 μg mL−1 for Mn3O4 NPs from P. dulcis leaf extract. In general, the phytosynthetic route with synergistic effect of nanohybrid demonstrated an interaction with cancer cells, highlighting a pioneering optimum approach in synthesis of Mn3O4 NPs from aerial parts of P. dulcis.

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Section: Resultssupporting

confidence: 87%

Biological synthesis of manganese oxide nanoparticles from aerial parts of Prunus dulcis and their in vitro investigation of medical properties

Aarthi,

Anitha

2023

Applied Organom Chemis

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“…The diffraction peaks were observed at 18.13°, 29.05°, 31.2°, 32.5°, 36.24°, 38.19°, 44.53°, 50.91°, 58.67°, 60.01°, and 64.8°, corresponding to the (101), (112), (200), (103), (211), (004), (220), (204), (321), (224), and (400) crystal planes of the Mn 3 O 4 , respectively (according to the JCPDS card No. 24-0734) [ 30 ].…”

Section: Resultsmentioning

confidence: 99%

“…The diffraction peaks were observed at 18.13 112), ( 200), ( 103), ( 211), (004), ( 220), ( 204), (321), (224), and (400) crystal planes of the Mn 3 O 4 , respectively (according to the JCPDS card No. 24-0734) [30].…”

Section: The Physical Properties Of N P-doped Mn 3 O 4 Materialsmentioning

confidence: 99%

“…The diffraction peaks were observed at 18.13• , 29.05 • , 31.2 • , 32.5 • , 36.24 • , 38.19 • , 44.53 • , 50.91 • , 58.67 • , 60.01 • , and 64.8 • , corresponding to the (101), (112), (200), (103), (211), (004), (220), (204), (321), (224), and (400) crystal planes of the Mn 3 O 4 , respectively (according to the JCPDS card No. 24-0734)[30].However, after chitosan was added to prepare the Mn 3 O 4 @C material and underwent carbonization, the diffraction peaks of the Mn 3 O 4 @C hybrid material became boarder and shifted a little to a lower 2θ, indicating that the Mn 3 O 4 @C electrode material had smaller particle sizes. There were no distinct diffraction peaks corresponding to the carbon crystals, indicating that carbon also existed in an almost amorphous form in the Mn 3 O 4 @C hybrid material.…”

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confidence: 99%

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Boosting the Capacitive Performance of Supercapacitors by Hybridizing N, P-Codoped Carbon Polycrystalline with Mn3O4-Based Flexible Electrodes

Kang¹,

Yang²

2023

Nanomaterials

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Chitosan, a biomass raw material, was utilized as a carbon skeleton source and served as a nitrogen (N) atom dopant in this study. By co-doping phosphorus (P) atoms from H3PO4 and nitrogen (N) atoms with a carbon (C) skeleton and hybridizing them with Mn3O4 on a carbon fiber cloth (CC), an Mn3O4@NPC/CC electrode was fabricated, which exhibited an excellent capacitive performance. The N, P-codoped carbon polycrystalline material was hybridized with Mn3O4 during the chitosan carbonization process. This carbon polycrystalline structure exhibited an enhanced conductivity and increased mesopore content, thereby optimizing the micropore/mesopore ratio in the electrode material. This optimization contributed to the improved storage, transmission, and diffusion of electrolyte ions within the Mn3O4@NPC electrode. The electrochemical behavior was evaluated via cyclic voltammetry and galvanostatic charge–discharge tests using a 1 M Na2SO4 electrolyte. The capacitance significantly increased to 256.8 F g−1 at 1 A g−1, and the capacitance retention rate reached 97.3% after 5000 charge/discharge cycles, owing to the higher concentration of the P-dopant in the Mn3O4@NPC/CC electrode. These findings highlight the tremendous potential of flexible supercapacitor electrodes in various applications.

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Green Synthesis of Chlorophyta Seaweed Mediated Mn ₃ O ₄ Nanoparticles: Electrochemical Applications and Evaluation of Capacitive and Diffusive Contributions

Darboe,

Agyemang,

Hou Gbologah

et al. 2024

Analytical Letters

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Sketchy synthesis of Mn3O4, Mn3O4/AC and Mn3O4/CNT composites for application of/in energy cache

Cited by 4 publications

References 17 publications

Biological synthesis of manganese oxide nanoparticles from aerial parts of Prunus dulcis and their in vitro investigation of medical properties

Biological synthesis of manganese oxide nanoparticles from aerial parts of Prunus dulcis and their in vitro investigation of medical properties

Boosting the Capacitive Performance of Supercapacitors by Hybridizing N, P-Codoped Carbon Polycrystalline with Mn3O4-Based Flexible Electrodes

Green Synthesis of Chlorophyta Seaweed Mediated Mn ₃ O ₄ Nanoparticles: Electrochemical Applications and Evaluation of Capacitive and Diffusive Contributions

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Sketchy synthesis of Mn3O4, Mn3O4/AC and Mn3O4/CNT composites for application of/in energy cache

Cited by 4 publications

References 17 publications

Biological synthesis of manganese oxide nanoparticles from aerial parts of Prunus dulcis and their in vitro investigation of medical properties

Biological synthesis of manganese oxide nanoparticles from aerial parts of Prunus dulcis and their in vitro investigation of medical properties

Boosting the Capacitive Performance of Supercapacitors by Hybridizing N, P-Codoped Carbon Polycrystalline with Mn3O4-Based Flexible Electrodes

Green Synthesis of Chlorophyta Seaweed Mediated Mn 3 O 4 Nanoparticles: Electrochemical Applications and Evaluation of Capacitive and Diffusive Contributions

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Green Synthesis of Chlorophyta Seaweed Mediated Mn ₃ O ₄ Nanoparticles: Electrochemical Applications and Evaluation of Capacitive and Diffusive Contributions