This paper is concerned with the ultimate behaviour of lightly reinforced concrete floor slabs under extreme loading conditions. Particular emphasis is given to examining the failure conditions of idealised composite slabs which become lightly reinforced in a fire situation due to the early loss of the steel deck. An experimental study is described which focuses on the response of two-way spanning floor slabs with various material and geometric configurations. The tests enable direct assessment of the influence of a number of key parameters such as the reinforcement type, properties and ratio on the ultimate response. The results also permit the development of simplified expressions, which capture the influence of salient factors such as bond characteristics and reinforcement properties, for predicting the ductility of lightly reinforced floor slabs. The companion paper complements the experimental observations with detailed numerical assessments of the ultimate response, and proposes analytical models which predict failure of slab members by either reinforcement fracture or compressive crushing of concrete.