2009
DOI: 10.2478/s11532-009-0022-2
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Sol-gel bioactive glass-ceramics Part I: Calcium phosphate silicate/wollastonite glass-ceramics

Abstract: Abstract:In this work we present experimental results about synthesis, structure evolution and in vitro bioactivity of new calcium phosphate silicate/wollastonite (CPS/W) glass-ceramics. The samples obtained were synthesized via polystep sol-gel process with different Ca/P+Si molar ratio (R). The structure of the materials obtained was studied by XRD, FTIR spectroscopy and SEM. XRD showed the presence of Ca 15 (PO 4 ) 2 (SiO 4 ) 6 , β-CaSiO 3 and α-CaSiO 3 for the sample with R=1.89 after thermal treatment at … Show more

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Cited by 16 publications
(14 citation statements)
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“…3-, Si-O-Si or may be CH 3 groups in the less hydrated acetates [9,23]. Briefly, from the presented FTIR results, we concluded that the presented FTIR data are in accordance to XRD results.…”
Section: Results and Discussionanalysis Of The Composites Before In Vsupporting
confidence: 77%
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“…3-, Si-O-Si or may be CH 3 groups in the less hydrated acetates [9,23]. Briefly, from the presented FTIR results, we concluded that the presented FTIR data are in accordance to XRD results.…”
Section: Results and Discussionanalysis Of The Composites Before In Vsupporting
confidence: 77%
“…% P 2 O 5 . The procedure for the synthesis and evaluation of the structure of the prepared CPS ceramics was described in our previous work [9]. Collagen type I, taken in amounts corresponding to the composite content was diluted in 15 ml CH 3 COOH for 24 h at room temperature under intensively stirring.…”
Section: Experimental Part Preparation Of the Compositesmentioning
confidence: 99%
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“…Asymmetric stretching vibration of phosphate (PO 4 3− ) was identified at 600 cm −1 [19,26]. A weak band at ≈940 cm −1 , assigned to symmetric stretching of silicate [17] and overlapping PO 4 , was detected in liquid of both materials [17,28] (Figure 1(a)). …”
Section: Fourier Transform Infraredmentioning
confidence: 99%