2023
DOI: 10.1021/jacs.3c00258
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Solid-State Synthesis of Aluminophosphate Zeotypes by Calcination of Amorphous Precursors

Abstract: Because of the growing interest in the applications of zeolitic materials and the various challenges associated with traditional synthesis methods, the development of novel synthesis approaches remains of fundamental importance. Herein, we report a general route for the synthesis of aluminophosphate (AlPO) zeotypes by simple calcination of amorphous precursors at moderate temperatures (250–450 °C) for short reaction times (3–60 min). Accordingly, highly crystalline AlPO zeotypes with various topologies of AST,… Show more

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Cited by 6 publications
(2 citation statements)
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“…And the materials usually possess poor structure stability and ecological adaptiveness resulting from smaller grain sizes. , For example, Xie et al reported worse structure stability of CoS 2 synthesized hydrothermally, with decomposition occurring at ∼300 °C. Unlike the hydrothermal method, solid-phase sintering is a process of transition from the metastable phase to the stable phase of the minimum free energy, which helps to obtain thermodynamically stable materials, with large-scale manufacturing. , Nevertheless, it is difficult to obtain a single-phase structure without impurities by this sintering, especially within a high-doping content. For instance, Hu et al synthesized Fe 0.5 Co 0.5 S 2 by solid-phase and liquid-phase process, where the former was impure phase while the latter was pure phase.…”
Section: Introductionmentioning
confidence: 99%
See 1 more Smart Citation
“…And the materials usually possess poor structure stability and ecological adaptiveness resulting from smaller grain sizes. , For example, Xie et al reported worse structure stability of CoS 2 synthesized hydrothermally, with decomposition occurring at ∼300 °C. Unlike the hydrothermal method, solid-phase sintering is a process of transition from the metastable phase to the stable phase of the minimum free energy, which helps to obtain thermodynamically stable materials, with large-scale manufacturing. , Nevertheless, it is difficult to obtain a single-phase structure without impurities by this sintering, especially within a high-doping content. For instance, Hu et al synthesized Fe 0.5 Co 0.5 S 2 by solid-phase and liquid-phase process, where the former was impure phase while the latter was pure phase.…”
Section: Introductionmentioning
confidence: 99%
“…20,21 For example, Xie et al 22 sintering is a process of transition from the metastable phase to the stable phase of the minimum free energy, which helps to obtain thermodynamically stable materials, with large-scale manufacturing. 23,24 Nevertheless, it is difficult to obtain a single-phase structure without impurities by this sintering, especially within a high-doping content. For instance, Hu et al 5 synthesized Fe 0.5 Co 0.5 S 2 by solid-phase and liquid-phase process, where the former was impure phase while the latter was pure phase.…”
Section: Introductionmentioning
confidence: 99%