Solvent-assisted dispersive liquid-solid phase extraction of organophosphorus pesticides using a polypyrrole thin film–coated porous composite magnetic sorbent prior to their determination with GC-MS/MS

Jullakan, Sirintorn; Bunkoed, Opas; Pinsrithong, Sakchaibordee

doi:10.1007/s00604-020-04649-1

Cited by 19 publications

(6 citation statements)

References 34 publications

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“…The method, solvent, extraction equipment, auxiliary extraction time, LOD, recovery, and instrument were compared to other determination methods of parathion-methyl 19,20,34–36 (Table 3). The proposed method uses a small volume of environmentally friendly extraction solvent.…”

Section: Resultsmentioning

confidence: 99%

Section: Comparison With Other Methodsmentioning

confidence: 99%

“…Current detection methods of parathion-methyl mainly involve gas chromatography, 19 high-performance liquid chromatography, 20 mass spectrometry, 21 and electrochemical methods. 22 However, expensive equipment, long analysis times, and well-trained operators are required.…”

Section: Introductionmentioning

confidence: 99%

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Density-adjusted liquid-phase microextraction with smartphone digital image colorimetry to determine parathion-methyl in water, fruit juice, vinegar, and fermented liquor

Jiang

Guo

et al. 2022

RSC Adv.

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Section: Resultsmentioning

confidence: 99%

Section: Comparison With Other Methodsmentioning

confidence: 99%

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Density-adjusted liquid-phase microextraction with smartphone digital image colorimetry to determine parathion-methyl in water, fruit juice, vinegar, and fermented liquor

Jiang

Guo

et al. 2022

RSC Adv.

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“…23,24 Therefore, the detection and monitoring of OPs is of significance. Although many instrumentation and sensing methods have been developed for OP detection, [25][26][27][28] the hydrogel SERS chip shows many advantages such as low cost, high sensitivity, rapid detection, and high-throughput. These satisfactory results suggest that the developed hydrogel SERS chip shows great potential in on-site trace analysis for food safety, environmental monitoring, and homeland security.…”

Section: Introductionmentioning

confidence: 99%

Hybridizing aggregated gold nanoparticles with a hydrogel to prepare a flexible SERS chip for detecting organophosphorus pesticides

Zhang

Zhu

Chen

et al. 2022

Analyst

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“…An alternative strategy that also improved the extraction efficiency of PAHs is a recently reported extraction technique that combined a liquid phase and a porous solid phase [19]. Using this technique, PAHs could be extracted from the sample solution based on the partition between the liquid phase, which is the extraction solvent, and the surface of the solid phase sorbent.…”

Section: Introductionmentioning

confidence: 99%

A hierarchical porous composite magnetic sorbent of reduced graphene oxide embedded in polyvinyl alcohol cryogel for solvent‐assisted‐solid phase extraction of polycyclic aromatic hydrocarbons

Rattanakunsong

Jullakan

Płotka‐Wasylka

et al. 2022

J of Separation Science

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A hierarchical porouscomposite magnetic sorbent was fabricated and applied to the dispersive solvent‐assisted solid‐phase extraction of five polycyclic aromatic hydrocarbons. A sorbent was first prepared by incorporating graphene oxide, calcium carbonate, and magnetite nanoparticles into a polyvinyl alcohol cryogel. The graphene oxide was converted to reduced graphene oxide using ascorbic acid and a hierarchical porous structure was produced by reacting hydrochloric acid with incorporated calcium carbonate to generate carbon dioxide bubbles which created a second network. Before extracting the target analytes, the extraction solvent was introduced into the hierarchical pore network of the sorbent. The extraction was based on the partition between the analytes and introduced extraction solvent and the adsorption of analytes on reduced graphene oxide.The extraction efficiency was enhanced through π‐π and hydrophobic interactions between polycyclic aromatic hydrocarbons and reduced graphene oxide and extraction solvent. The extracted polycyclic aromatic hydrocarbons were determined by using high‐performance liquid chromatography coupled with a fluorescence detector. The developed method was applied to extract polycyclic aromatic hydrocarbons in disposable diaper, coffee, and tea samples and recoveries from 84.5 to 99.4% were achieved with relative standard deviations below 7%. The developed sorbent exhibited good reproducibility and could be reused for 10 cycles.The developed sorbent exhibited good reproducibility and could be reused for 10 cycles.The developed sorbent exhibited good reproducibility and could be reused for 10 cycles.

show abstract

Solvent-assisted dispersive liquid-solid phase extraction of organophosphorus pesticides using a polypyrrole thin film–coated porous composite magnetic sorbent prior to their determination with GC-MS/MS

Cited by 19 publications

References 34 publications

Density-adjusted liquid-phase microextraction with smartphone digital image colorimetry to determine parathion-methyl in water, fruit juice, vinegar, and fermented liquor

Density-adjusted liquid-phase microextraction with smartphone digital image colorimetry to determine parathion-methyl in water, fruit juice, vinegar, and fermented liquor

Hybridizing aggregated gold nanoparticles with a hydrogel to prepare a flexible SERS chip for detecting organophosphorus pesticides

A hierarchical porous composite magnetic sorbent of reduced graphene oxide embedded in polyvinyl alcohol cryogel for solvent‐assisted‐solid phase extraction of polycyclic aromatic hydrocarbons

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