Publication information
Journal of Materials Processing Technology, 211 (7): 1210-1216Publisher Elsevier Item record/more information http://hdl.handle.net/10197/5260
Publisher's statementThis is the author's version of a work that was accepted for publication in Journal of Materials Processing Technology. Changes resulting from the publishing process, such as peer review, editing, corrections, structural formatting, and other quality control mechanisms may not be reflected in this document. Changes may have been made to this work since it was submitted for publication. A definitive version was subsequently published in Journal of Materials Processing Technology, 211 (7)
AbstractThere is considerable interest in processing technologies which can lead to more energy efficient sintering of abrasive metal matrix composites. In this study the use of a novel microwave plasma processing technique called Rapid Discharge Sintering (RDS) for sintering nickel-diamond metal matrix composites (MMCs) is evaluated. Nickel-diamond powder composites (80 -20 % by weight respectively) were uniaxially pressed into 20 mm discs at compaction pressures of 100, 200 and 300 MPa. The discs were sintered using a microwave plasma formed with hydrogen and hydrogen/nitrogen as the discharge gases. For comparison, discs were also sintered using a tube furnace in a gas flow of hydrogen and nitrogen (3:1). Discs pressed to 300 MPa were treated at both 850 and 1000 o C. The properties of the sintered nickel-diamond composites were characterised using density, flexural stress, hardness, wear resistance, SEM and XRD. The RDS samples sintered at 1000 o C achieved the maximum disc strength of approximately 470 MPa within a 20 minute chamber processing time, compared with 6 hours for furnace sintered samples. RDS samples exhibited increased hardness values and a finer nickel matrix over furnace sintered samples. RDS has shown the ability to process nickel-diamond MMCs without oxidation or graphitisation at higher temperatures. As a result, minimal diamond destruction was observed during abrasive wear testing for RDS samples.