Abstract. Nanoparticle synthesis was performed using high-powered pulsemodulated induction thermal plasma (PMITP) technique to study the effect of coil current modulation on synthesized nanoparticles. This is the first paper to present a summary of results of TiO 2 nanoparticle synthesis using high-power Ar-O 2 PMITP at 20 kW. The synthesized particles were analyzed using a field emission scanning electron microscope (FE-SEM), and X-ray diffractometry (XRD). In addition, optical emission spectroscopy (OES) was used during nanoparticle synthesis experiments to measure TiO spectra and to determine the time-averaged vibrational and rotational temperatures of TiO in the reaction chamber. Results showed that the PMITP produced smaller nanoparticles and a narrower size distribution of particles. Moreover, PMITP provided a lower-temperature region in the reaction chamber downstream of the plasma torch than such regions in non-modulated thermal plasmas.