HE AIM of this greenhouse research is to optimize the use of agricultural waste by recycling it into organic fertilizer (compost). Furthermore, to increase the effectiveness of the compost produced, agricultural waste is treated with soil amendments, specifically sulfur (S) and gypsum (G), and nanotechnology is used to increase its activity and reactivity with various soil components. Convert to nano fraction (N-form). The investigation encompassed the analysis of chemical properties (pH, electrical conductivity (EC), organic matter (OM), total nitrogen, and available nutrients) and Fourier-transform infrared spectroscopy (FTIR) spectra (functional groups). Furthermore, the impact of compost, in various types and forms, on the content of available nutrients in saline soils. The results demonstrated significant variations in the chemical composition and functional group content of the produced composts, influenced by the additive type and compost size fractions. These treatments led to increased levels of OM, available nutrients, even with a decrease in compost pH. Consequently, these interventions accelerated the decomposition rate of agricultural wastes, resulting in improved compost properties. This enhancement amplified the beneficial effects of the used composts as amendments and vital resources for essential plant nutrients, as evidenced by notable increases in soil contents of available nitrogen, phosphorus, potassium, and sulfur.