2024
DOI: 10.3390/molecules29122721
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Structural Characterization and Electrochemical Studies of Selected Alkaloid N-Oxides

Olha Dushna,
Liliya Dubenska,
Andrzej Gawor
et al.

Abstract: In this work, we synthesized and confirmed the structure of several alkaloid N-oxides using mass spectrometry and Fourier-transform infrared spectroscopy. We also investigated their reduction mechanisms using voltammetry. For the first time, we obtained alkaloid N-oxides using an oxidation reaction with potassium peroxymonosulfate as an oxidant. The structure was established based on the obtained fragmentation mass spectra recorded by LC-Q-ToF-MS. In the FT-IR spectra of the alkaloid N-oxides, characteristic s… Show more

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