Structural, Microstructural and Magnetic Characterizations of Mechanically Alloyed Fe65Si20Cr15 Powders Mixture

Ammouchi, N.; Otmani, A.; Bensebaa, Z.; Azzaza, S.; Bououdina, M.; Djekoun, A.; Bechiri, L.; Grenèche, Jean‐Marc

doi:10.1007/s10948-015-3203-6

Cited by 5 publications

(1 citation statement)

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“…These materials can thus be presented in various forms according to the dimensionality of the nanostructured character [7]. We can distinguish nanoparticles, thin and multilayer lms, nanostructured powders (micron particles made up of nanometric grains), nanocrystalline alloys (crystalline nanograins within an amorphous metallic matrix), clusters dispersed in a matrix, etc [8][9][10]. Due to the con nement effect, these materials conceal a signi cant atomic proportion included in surfaces (nanoparticles), interfaces (multilayers, nanocrystalline) and within grain boundaries (nanostructured powders); they possess physical properties by consequent very different from those of microcrystalline or massive materials.…”

Section: Introductionmentioning

confidence: 99%

Investigating on structural, microstructural and magnetic properties of nanocrystalline Fe60Al35Mg5 alloy synthesized by high energy ball milling

Hafs¹,

Hafs

Berdjane

et al. 2023

Preprint

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The mechanical alloying process has been used to synthesise the nanocrystalline Fe60Al35Mg5 ( wt % )powders in a high energy planetary ball-mill Retsch PM 400. The evolution structural, microstructural and magnetic properties of ball-milled powders at different milling times (t variation from 0 to 32 h) were investigated by X-ray diffraction using the MAUD program which is based on the Rietveld method and the vibrating sample magnetometer (VSM). The XRD results reveal the formation of a bcc-Fe (Al, Mg) solid solution after 8 h of milling possessing a lattice parameter of 0,2895nm after 32 h of milling. It is also observed a refinement of the grain size which reaches 18,75 nm, and an increase in the microstrain after 32 hours of milling. Magnetic measurements of the milled Fe60Al35Mg5 ( wt % ) powder mixture exhibit a soft ferromagnetic character where the magnetic parameters are found to be very sensitive to the milling time mainly due to the particle size refinement as well as the formation of the solid solutions.

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