2011
DOI: 10.1134/s0022476611030292
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Structural studies of 3-chloro-N-(8′-quinolyl)×benzo[b]thiophene-2-carboxamide

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“…Ni/Co-MOF was synthesized through a hydrothermal method according to the reported approach. 30,31 An equimolar amount of Co(NO 3 ) 2 Á6H 2 O solution and Ni(NO 3 ) 2 Á6H 2 O (1 mmol) was mixed with an equimolar amount of terephthalic acid and pyrazine solution (2 mmol) in H 2 O (14 ml) and the obtained solution was kept at 200 1C for 48 h in a 23 ml Teflon-lined stainless steel autoclave and then cooled at 5 1C h À1 to room temperature. The obtained crystals were washed with distilled water to remove the unreacted substances and dried at room temperature.…”
Section: Methodsmentioning
confidence: 99%
“…Ni/Co-MOF was synthesized through a hydrothermal method according to the reported approach. 30,31 An equimolar amount of Co(NO 3 ) 2 Á6H 2 O solution and Ni(NO 3 ) 2 Á6H 2 O (1 mmol) was mixed with an equimolar amount of terephthalic acid and pyrazine solution (2 mmol) in H 2 O (14 ml) and the obtained solution was kept at 200 1C for 48 h in a 23 ml Teflon-lined stainless steel autoclave and then cooled at 5 1C h À1 to room temperature. The obtained crystals were washed with distilled water to remove the unreacted substances and dried at room temperature.…”
Section: Methodsmentioning
confidence: 99%