Structure and mechanical properties of β-TCP scaffolds prepared by ice-templating with preset ice front velocities

Flauder, Stefan; Gbureck, Uwe; Müller, Frank A.

doi:10.1016/j.actbio.2014.08.020

Cited by 49 publications

(62 citation statements)

References 31 publications

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“…Color code: blue: no defects [26–31, 33, 36, 38, 40, 41, 43, 44, 46, 50–55, 61, 64, 65, 67, 68, 70, 71, 73, 77, 78, 85, 90, 91, 94, 98, 100, 103–110, 113, 115, 118, 124–127, 129, 130, 132, 134, 135, 143], yellow: defects [25, 52, 86, 91, 96], white: cannot tell from the published micrographs [37, 39, 49, 56, 91, 95, 96, 119]. …”

Section: Resultsmentioning

confidence: 99%

“…Data from references [26–28, 31, 36–39, 46, 49, 51–53, 56, 61, 64, 65, 67, 68, 70, 71, 73, 77, 78, 85, 94–96, 103–106, 113, 118, 119, 125–127, 129, 130, 132]. …”

Section: Resultsmentioning

confidence: 99%

“…References for the data: water [8, 12, 26, 27, 31, 33–38, 43–49, 51, 52, 55–61, 68, 69, 72–76, 81, 84, 86–92, 94–101, 103, 104, 111, 113, 116, 119, 124, 128–132, 134, 135], camphene [9, 29, 30, 42, 50, 64–67, 70, 80, 85, 93, 102, 105–109, 114, 115, 117, 118, 120–123, 125–127, 136], TBA [10, 32, 39–41, 53, 62, 63, 71, 77, 78, 82, 83, 110, 137]. The marker size is proportional to the pore size.…”

Section: Resultsmentioning

confidence: 99%

“…The papers analyzed cover a variety of materials including ceramics (alumina [8–11, 26, 28, 32, 36, 38, 43, 48, 54, 58, 77, 81, 89, 102, 104, 105, 111, 112, 131, 143], zirconia [49, 80, 100, 101, 103, 125–127], silicon carbide [45, 106, 130], silicon nitride [35, 69, 72, 75, 76, 79, 84, 87, 88, 128], mullite [90, 110, 124, 137], hydroxyapatite [12, 37, 44, 52, 61, 68, 78, 86, 91, 95–98, 107, 109, 113, 115, 120, 134, 135], tri-calcium phosphate [31, 40, 56, 117, 118], lead zirconate titanate (PZT) [39, 63, 74, 82, 83, 121, 122], barium titanate [73], silica/kaolinite [47], titania [24, 29, 50, 99], zirconium diboride [51], chromium carbide [42], sialon [64, 66], lithium iron phosphate [60], yttrium orthosilicate [57, 62], cermets [116, …”

Section: Methodsmentioning

confidence: 99%

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A meta-analysis of the mechanical properties of ice-templated ceramics and metals

Deville

Meille

Seuba

2015

Science and Technology of Advanced Materials

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Ice templating, also known as freeze casting, is a popular shaping route for macroporous materials. Over the past 15 years, it has been widely applied to various classes of materials, and in particular ceramics. Many formulation and process parameters, often interdependent, affect the outcome. It is thus difficult to understand the various relationships between these parameters from isolated studies where only a few of these parameters have been investigated. We report here the results of a meta analysis of the structural and mechanical properties of ice templated materials from an exhaustive collection of records. We use these results to identify which parameters are the most critical to control the structure and properties, and to derive guidelines for optimizing the mechanical response of ice templated materials. We hope these results will be a helpful guide to anyone interested in such materials.

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Section: Resultsmentioning

confidence: 99%

“…Data from references [26–28, 31, 36–39, 46, 49, 51–53, 56, 61, 64, 65, 67, 68, 70, 71, 73, 77, 78, 85, 94–96, 103–106, 113, 118, 119, 125–127, 129, 130, 132]. …”

Section: Resultsmentioning

confidence: 99%

Section: Resultsmentioning

confidence: 99%

Section: Methodsmentioning

confidence: 99%

See 2 more Smart Citations

A meta-analysis of the mechanical properties of ice-templated ceramics and metals

Deville

Meille

Seuba

2015

Science and Technology of Advanced Materials

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“…Recently, Flauder et al presented a study utilizing the exponential cooling function given by Stefan in ice‐templating processes and showed that the application of this cooling function leads to homogeneous pore sizes throughout the whole sample height of frozen ceramic suspensions . The present study focuses on the theoretical derivation, investigation, and discussion of this analytical cooling function.…”

Section: Introductionmentioning

confidence: 93%

Directional Solidification with Constant Ice Front Velocity in the Ice‐Templating Process

et al. 2015

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An exponential cooling function for the directional solidification of liquids with constant ice front velocities is investigated with respect to an enhanced control over the ice-templating process. It is mathematically derived and set into relation to other cooling functions found in literature. A theoretical limit of applicability is discussed and a mathematical expression for the maximum sample size realizable with this new approach is derived. Experimental results from the time-resolved direct measurement of the ice front evolution during the directional solidification of pure water and a ceramic b-tricalcium phosphate (b-TCP) suspension in a cooling room environment are presented. These results are compared to the results of numerical simulations. Ice front velocities from 10 to 50 mm s -1 are realized.

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Bone‐inspired Biomaterials

Müller

2018

Bioinspired Materials Science and Engineering

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Structure and mechanical properties of β-TCP scaffolds prepared by ice-templating with preset ice front velocities

Cited by 49 publications

References 31 publications

A meta-analysis of the mechanical properties of ice-templated ceramics and metals

A meta-analysis of the mechanical properties of ice-templated ceramics and metals

Directional Solidification with Constant Ice Front Velocity in the Ice‐Templating Process

Bone‐inspired Biomaterials

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