2002
DOI: 10.1016/s0144-8617(01)00164-3
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Study of a preparative-scale process for the production of amylose

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Cited by 45 publications
(36 citation statements)
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“…The molar mass, M, and the root-meansquare radius, r rms , were obtained by the Berry method [34,35] performing a first-order fit to data obtained at scattering angles of 60.0-121.2°(detectors [8][9][10][11][12][13][14]. The lowest scattering angles, 25.9°and 51.5°(detectors 4-7), were not included, as the data obtained was imprecise.…”
Section: Data Processingmentioning
confidence: 99%
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“…The molar mass, M, and the root-meansquare radius, r rms , were obtained by the Berry method [34,35] performing a first-order fit to data obtained at scattering angles of 60.0-121.2°(detectors [8][9][10][11][12][13][14]. The lowest scattering angles, 25.9°and 51.5°(detectors 4-7), were not included, as the data obtained was imprecise.…”
Section: Data Processingmentioning
confidence: 99%
“…Secondly, elevated temperatures [12] or severe shearing [13] used for Published in the topical collection Field-and Flow-based Separations with guest editors Gaetane Lespes, Catia Contado, and Bruce Gale. dissolution can cause molecular degradation of amylose.…”
Section: Introductionmentioning
confidence: 99%
“…The rate for heating and cooling was 10 K/min. The molar masses M n and M w of the used wrinkled pea starch were estimated as described in [9]. The amount of amylose was determined according to Richter et al [10].…”
Section: Instrumentationmentioning
confidence: 99%
“…In this paper the reactions of aliphatic isocyanates with wrinkled pea starch in homogeneous phase are described, catalysed by Lewis acids. The used isocyanates have linear alkyl chains with 7,9,11,15 or 18 carbon atoms. The formation of the starch carbamates in a reaction flask was intensively studied by variation of the length of alkyl chains of the isocyanates and the degrees of substitution of the starch carbamates.…”
Section: Introductionmentioning
confidence: 99%
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