The Shubnikov-de Haas effect in InAlAs measured using pulsed magnetic fields up to 50 T is reported. The InAlAs samples were grown by molecular beam epitaxy ͑MBE͒ and were either ␦ or slab doped with silicon at densities up to 7ϫ10 12 cm Ϫ2 . Comparison of experimental subband densities with those calculated self-consistently shows that spreading of Si occurs by surface segregation at growth temperatures of ϳ520°C, similar to its behavior in MBE-grown InGaAs. In contrast to InGaAs, the InAlAs exhibits persistent photoconductivity which appears to be caused by a bulk defect rather than DX͑Si͒ states. © 1999 American Institute of Physics.
͓S0021-8979͑99͒00423-5͔Shubnikov-de Haas ͑SdH͒ measurements combined with self-consistent calculations ͑SCC͒ have been used to estimate the spreading of Si as a function of growth temperature in ␦-and slab-doped InGaAs.1-3 However, the larger electron effective mass in InAlAs and its lower electron mobility mean that substantially higher magnetic fields are required to resolve the individual subbands for structures doped with comparable donor densities. In this communication, we report the observation of the SdH effect in InAlAs ␦ and slab doped with Si to densities of N Si ϳ7ϫ10 12 cm Ϫ2 . Pulsed magnetic fields up to 50 T were needed to measure peaks due to depopulation of the Landau levels of the iϭ0 subband. A comparison of the SdH data with SCC provides an estimate of Si spreading at growth temperatures T S around 520°C. Persistent photoconductivity ͑PPC͒ due to deep states in the InAlAs has been observed, and evidence is presented which rules against DX͑Si͒ centers as the cause.The Si ␦-and slab-doped InAlAs layers were grown lattice matched on Fe-InP͑100͒ by molecular beam epitaxy ͑MBE͒ in a constant As 2 flux of Ϸ2.0ϫ10 15 molecules cm Ϫ2 s
Ϫ1. The growth rate was 1.0 m/h and the growth temperature was varied between T S Ϸ460 and 520°C. A series of 0.5-2.0 m thick InGaAs layers doped uniformly with Si at concentrations ranging from 5ϫ10 16 to 4ϫ10 A 100 Å cap layer of un-InGaAs was grown to assist the formation of ohmic contacts on Hall bars with a 3:1 length to width ratio. The quantum transport measurements were carried out at 4.2 K with a 0-50 T pulsed magnetic field system 4 and at 1.2 K in a 0-13 T superconducting magnet. The electron subband densities n i ϭ2e i /h (iϭ0,1,2,...) were calculated from the peaks in the fast Fourier transform ͑FFT͒ spectra of the SdH data assuming, unresolved spin splitting. i is the magnetic frequency of the ith peak, e is the electron charge, and h is Planck's constant. For the PPC study, the samples were cooled to 4.2 K in the dark, illuminated with a red light emitting diode ͑LED͒ until the zero magnetic field longitudinal resistance stopped increasing, and then measured 1 and 14 h after illumination.Two representative samples, B689 and A1337, have been selected to illustrate the new data. B689 was grown entirely at T S ϳ520°C and was ␦ doped with N Si ϭ7ϫ10 12 cm Ϫ2 . A1337 was ␦ doped to ϳ5ϫ10 12 cm Ϫ2 and was also grown at 520°C,...