2015
DOI: 10.1016/j.matlet.2014.09.105
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Submicron diameter single crystal sapphire optical fiber

Abstract: Submicron diameter single crystal sapphire optical fiber, Materials Letters, http://dx. AbstractIn this work, a submicron-diameter single crystal sapphire optical fiber was demonstrated via wet acid etching at elevated temperatures. Etch rates on the order 2.3 μm/hr were achievable with a 3:1 molar ratio sulfuric-phosphoric acid solution maintained at a temperature of 343°C. A sapphire fiber with an approximate diameter of 800 nm was successfully fabricated from a commercially available fiber with an original … Show more

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Cited by 17 publications
(5 citation statements)
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“…For an air-clad sapphire FBG, the reflection peaks of different modes can be easily distinguished once the diameter is smaller than 20 μm and each peak has a <1 nm bandwidth [25]. The fabrication of a small diameter sapphire fiber can be achieved by laser-heated pedestal growth (LHPG) fabrication [28], in which diameters down to about 20 microns can be achieved, or by chemical-etching processing [29], in which diameters down to one micron or below can be achieved.…”
Section: Discussionmentioning
confidence: 99%
“…For an air-clad sapphire FBG, the reflection peaks of different modes can be easily distinguished once the diameter is smaller than 20 μm and each peak has a <1 nm bandwidth [25]. The fabrication of a small diameter sapphire fiber can be achieved by laser-heated pedestal growth (LHPG) fabrication [28], in which diameters down to about 20 microns can be achieved, or by chemical-etching processing [29], in which diameters down to one micron or below can be achieved.…”
Section: Discussionmentioning
confidence: 99%
“…The etching method employed has been described in greater detail previously [12]. In this work, the temperature profile of a typical etching session appeared as illustrated by Figure 4 below, where the solution reached its peak temperature of just over 340 • C over the course of about 2 h, after which etching was allowed to continue at a steady temperature for 8-10 h. As the acid solution was heated, several transformations took place due to heat and dehydration into diacid and polyacid forms, the nuances and impacts of which have been discussed elsewhere [15][16][17][18].…”
Section: Etching Behaviormentioning
confidence: 99%
“…We previously demonstrated a wet-acid etching method which was successfully applied to reduce the diameter of a sapphire optical fiber to less than 800 nm while maintaining a smooth, consistent surface [12]. This method, which summarily prescribes the immersion of sapphire fiber into a mixture of sulfuric and phosphoric acids at temperatures exceeding 340 • C, was employed again in the work presented below to produce an air-clad sapphire optical fiber demonstrating support of only the fundamental LP 01 mode at wavelengths of 783 nm and greater.…”
Section: Introductionmentioning
confidence: 99%
“…Compared to silica fiber, sapphire SCF is a better platform for supercontinum generation due to its high transparency up to 5 μm, low material dispersion in the 0.8 -5 μm spectral range, and higher laser damage threshold [6,7]. Furthermore, SCF-based sensors are the unique and effective solution in high-temperature, high-pressure, and chemically aggressive environments that require high temperature stability and transient response characteristics because of their high melting point, superb mechanical properties, and stable physical and chemical properties [8][9][10][11].…”
Section: Introductionmentioning
confidence: 99%