Sugar Functionalized Coumarin Motifs: Synthesis and Applications

Dwivedi, Shubhi; Dey, Soumyadip; Sau, Abhijit

doi:10.1016/j.carres.2024.109244

Carbohydrate Research

2024

DOI: 10.1016/j.carres.2024.109244

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Sugar Functionalized Coumarin Motifs: Synthesis and Applications

Shubhi Dwivedi,

Soumyadip Dey,

Abhijit Sau

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2024

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Benzene-1,3-disulfonyl Fluoride Mediated Synthesis of Glycosyl Fluorides from Glycosyl Hemiacetals

Dey,

Dwivedi,

Giri

et al. 2024

Org. Lett.

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We developed an efficient method for synthesizing glycosyl fluorides from glycosyl hemiacetals using benzene-1,3-disulfonyl fluoride (S2) as the fluorinating agent in combination with the base DBU (1,8-diazabicyclo[5.4.0]undec-7-ene) under mild conditions. This approach enabled the successful synthesis of 17 glycosyl fluorides with various functional groups, including disaccharides and deoxysulfates, with yields of up to 99%. The utility of these synthesized glycosyl fluorides was further demonstrated in the synthesis of important O-and Cglycosides.

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Benzene-1,3-disulfonyl Fluoride Mediated Synthesis of Glycosyl Fluorides from Glycosyl Hemiacetals

Dey,

Dwivedi,

Giri

et al. 2024

Org. Lett.

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show abstract

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Sugar Functionalized Coumarin Motifs: Synthesis and Applications

Cited by 1 publication

References 78 publications

Benzene-1,3-disulfonyl Fluoride Mediated Synthesis of Glycosyl Fluorides from Glycosyl Hemiacetals

Benzene-1,3-disulfonyl Fluoride Mediated Synthesis of Glycosyl Fluorides from Glycosyl Hemiacetals

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