ii ACKNOWLEDGEMENTS Thanks to J.A. Gilotti for primary advising and funding for this MS project.Much appreciation to W.C. McClelland for U-Pb geochronology of sample 14-33. L.E.Webb was vital for interpretation of Ar apparent age spectra and further advising of the 40 Ar/ 39 Ar geochronological method. D.A. Jones was invaluable in mineral separation of micas and in Ar lab instruction during my visit to the University of Vermont. K. Piepjohn is thanked for his digitized outcrop sketches. Lastly, L.K. Horkley was vital in SEM instruction, EMP geochemical data acquisition and creation of chemical X-ray maps. iii ABSTRACT This thesis presents 40 Ar/ 39 Ar geochronological analyses of biotite from thin ductile shear zones in Paleoproterozoic granulite-facies gneisses from the Ellesmere-Devon crystalline terrane, Nunavut, Canada. The gneisses are part of the Paleoproterozoic Thelon tectonic zone. U-Pb dates of zircon show that the gneisses have magmatic protolith ages ranging from 2007-1958 Ma. The quartzofeldspathic gneisses in southeast Ellesmere Island display centimeter-scale E-to NE-striking sinistral and dextral mylonite zones offsetting pegmatitic dikes that are the last stage of ductile deformation of the basement rocks. Samples were taken from nearshore outcrops at Hayes Fiord, Pim Island, NE of the Leffert Glacier and NW of Cape Isabella. Biotite clusters replace orthopyroxene as the result of post-granulite facies metamorphism in the gneisses. Biotite in mylonitic and ultramylonitic fabrics is found as flattened clusters and also as individual crystals defining shear bands related to mylonitization. Eight samples were dated, including biotite from five mylonites, one deformed pegmatite, one tonalite and muscovite from a pegmatite. Major element X-ray maps demonstrate that the biotite is chemically homogenous. Backscattered electron images and electron dispersive spectroscopy via scanning electron microscopy confirm that biotite lacks intercrystalline layering with other K phases. Step-heating analysis of mica at the University of Vermont yielded Paleoproterozoic 40 Ar/ 39 Ar ages. The apparent age spectra form plateau ages in all but one mylonite sample. Biotite from a protomylonite was 2051 ± 26 Ma, older than the protolith ages obtained from U-Pb zircon geochronology, and most likely indicates excess Ar. Pegmatitic muscovite was 1977 ± 35 Ma. Biotite dates range from 1874 ± 13 Ma to 1838 ± 14 Ma for the five mylonites without excess Ar. Biotite dated from ductile iv shear zones signals the latest deformation in the basement, which was active as early as 1887 Ma. v PUBLIC ABSTRACT I present a dating analysis of the mineral biotite from thin ductile shear zones in Precambrian gneisses from Ellesmere Island. Basement rocks in southeastern Ellesmere Island display centimeter-scale E-to NE-oriented, left-and right-lateral shear zones. Biotite clusters replace orthopyroxene as the result of post granulitefacies metamorphism in the gneisses. Biotite in highly deformed and recrystallized planar fabrics (i.e. mylo...