Iron is an important sheath material for fabrication of MgB 2 wires. However, the effect of Fe doping on the superconducting properties of MgB 2 remains controversial. In this work, we present results of nanoscale Fe particle doping in to MgB 2 . The Fe doping experiments were performed using both bulk and thin film form. It was found that Fe doping did not affect the lattice parameters of MgB 2 , as evidenced by the lack of change in the XRD peak positions for MgB 2 . Because of the high reactivity of nano-scale Fe particles, Fe doping is largely in the form of FeB at low doping level while Fe 2 B was detected at 10wt% doping by both XRD and TEM. There is no evidence for Fe substitution for Mg. The transition temperature decreased modestly with increasing Fe doping levels. The J c (H) performance was severely depressed at above 3wt% doping level. The detrimental effect of nano-scale Fe doping on both T c and J c (H) is attributable to the grain decoupling as a result of magnetic scattering of Fe-containing dopants at grain boundaries.