2022
DOI: 10.1039/d2nr02858a
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Symmetry and spacing controls in periodic covalent functionalization of graphite surfaces templated by self-assembled molecular networks

Abstract: We herein present the periodic covalent functionalization of graphite surfaces, creating a range of patterns of different symmetries and pitches at the nanoscale. Self-assembled molecular networks (SAMNs) of rhombic-shaped bis(dehydrobenzo[12]annulene)...

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Cited by 2 publications
(14 citation statements)
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“…All STM observations were performed at 20–25 °C using Nanoscope IIID or V (Bruker AXS) with an external pulse/function generator (Agilent 33220A), or PicoSPM (Agilent Technologies) with negative sample bias. STM tips were mechanically cut from Pt/Ir wire (80/20%, diameter 0.25 mm). All STM images were taken in a quasi-constant current mode.…”
Section: Methodsmentioning
confidence: 99%
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“…All STM observations were performed at 20–25 °C using Nanoscope IIID or V (Bruker AXS) with an external pulse/function generator (Agilent 33220A), or PicoSPM (Agilent Technologies) with negative sample bias. STM tips were mechanically cut from Pt/Ir wire (80/20%, diameter 0.25 mm). All STM images were taken in a quasi-constant current mode.…”
Section: Methodsmentioning
confidence: 99%
“…OA was used as the solvent after distillation. The sample solution (20–40 μL) was added to a homemade liquid cell placed on a highly oriented pyrolytic graphite surface (HOPG, grade ZYB, Momentive Performance Material Quartz, Inc., Strongsville, OH). We employed a liquid cell to minimize the effect of solvent evaporation. After annealing treatment at 80 °C for 3 h, the substrate was naturally cooled to room temperature.…”
Section: Methodsmentioning
confidence: 99%
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