Synthesis and characterization of a new organic sulphate, [2,3-(CH3)2C6H3NH3]HSO4·H2O

Synthesis, Structural Characterization and Thermal Behavior of New Organic–Inorganic Sulfate

“…According the detailed geometry of anionic entities, we note that the average values of the S-O distances and the O-S-O angles are 1.467(2) Å and 109.33(1)°, respectively. These results have been observed in other crystal structures [18]. In this structure the distances between two adjacent sulfur atom is S-S = 4.554 Å as would be expected in such compound [19].…”

Physico-chemical study of new supramolecular-architectured hybrid organic–inorganic sulfates incorporating diammoniumdiphenylsulfone cations

“…These different attributions, gathered in Table S12 (ESI †) do agree with those of the rst presented compound as well as with similar systems, taking into consideration the different vibrational effects and distances. [52][53][54][55] 3.4. 13 C nuclear magnetic resonance Nuclear magnetic resonance (NMR) is one of the most powerful spectroscopic techniques used to determine the structure of both organic and inorganic species.…”