Synthesis and characterization of composite magnetic microspheres of artemisia seed gum and chitosan

Abstract

In this study, composite magnetic microspheres of artemisia seed gum and chitosan were prepared in a well-shaped spherical form with a size range of 230-460 mm by the suspension crosslinking technique for use in the application of magnetic carrier technology. The magnetic material used in the preparation of the composite microspheres was prepared by precipitation from FeCl 3 and FeSO 4 solution in basic medium. The morphological, magnetic properties, and the functional groups of the microspheres were characterized by different techniques (i.e., SEM, magnetometry, and FTIR). The results demonstrated that the stirring rate of the suspension and the Fe 3 O 4 /chitosan ratio are the most effective parameters for the average of the size distributions and the magnetic quality of the microspheres, while the amount of artemisia seed gum and Tween-80 have no significant effect on these properties. The best magnetic quality of the composite magnetic microspheres is around 4.08 emu/g microspheres at 10 KG magnetic field intensity. The thermal stability of the composite magnetic microspheres was measured by using DSC methods.

Preparation of chitosan‐coated magnetite nanoparticles and application for immobilization of laccase

“…Chitosan based materials are used as supports, in various forms such as powder, flake, and gel, and of different geometrical configurations, for immobilization of several enzymes 11–15. Also, in the last decades, chitosan containing magnetic supports, especially magnetic microspheres16–18 were investigated for enzyme immobilization by using physical and chemical immobilization techniques 19, 20…”