2024
DOI: 10.1007/s00289-024-05241-w
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Synthesis and characterization of graft copolymer hydrogel by “grafting from” atom transfer radical polymerization using brominated macro monomeric initiator and investigation of hydrogel properties

Melahat Göktaş,
Ümran Aslan

Abstract: In this study, poly(ɛ-caprolactone-g-2-hydroxy ethyl methacrylate) [P(CL-g-HEMA)] graft copolymer hydrogels were successfully synthesized through multi-step reactions. For this purpose, firstly, hydroxyl-terminated poly(ɛ-caprolactone) (PCL-OH) was obtained by ring-opening polymerization (ROP) method of ɛ-caprolactone using 3-chlor-1,2-propanediol initiator, which is suitable for ring-opening polymerization method. Then, from the reaction of synthesized PCL-OH and 3-bromopropionyl chloride, a new brominated po… Show more

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