“…Metal alloys and oxide nanocomposites containing Fe dispersed in ceramic matrices have been of great interest in the scientific community since these materials have a variety of applications [1,2] such as contrast enhancement in magnetic resonance images, gas sensors, magnetic fluids, magnetocaloric applications, magneto-optical data storage devices, magnetically separable adsorbents, among others [2][3][4][5]. The determining aspects in the physicochemical properties of these composites are related to the particle size distribution, morphology of particles, defects, purity of phases, and the fraction of atoms present on the surface compared to bulk atoms and the chemistry of the surface [2,6]. The main challenges are related to the synthesis of nanocomposites with defined shape, controlled composition, and adjustable interparticle distance [7].…”