2004
DOI: 10.1016/j.matlet.2003.10.006
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Synthesis and characterization of mesoporous TiO2 with anatase wall

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Cited by 40 publications
(18 citation statements)
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“…It has been shown to produce crystalline TiO 2 nanocrystals with a narrow size distribution in the range of 4-5nm [43]. 15 The hydrothermal treatment method used in this experiment, appears to have a marked impact on the size of the anatase crystals, with those prepared in the microwave displaying average diameters of 5nm, 4nm less than those prepared in the oven. Hydrothermal treatment is a key parameter which can be altered to tailor crystal sizes.…”
Section: Hydrothermal Treatmentmentioning
confidence: 83%
See 1 more Smart Citation
“…It has been shown to produce crystalline TiO 2 nanocrystals with a narrow size distribution in the range of 4-5nm [43]. 15 The hydrothermal treatment method used in this experiment, appears to have a marked impact on the size of the anatase crystals, with those prepared in the microwave displaying average diameters of 5nm, 4nm less than those prepared in the oven. Hydrothermal treatment is a key parameter which can be altered to tailor crystal sizes.…”
Section: Hydrothermal Treatmentmentioning
confidence: 83%
“…The most attractive process for the synthesis of TiO 2 nanoparticles is the solgel method [7][8][9][10][11][12][13][14][15][16][17][18][19]. This process involves the hydrolysis and polycondensation of a metal alkoxide Ti(OR) 4 (R=alkyl groups) precursor and subsequent formation of a gel, which after heat treatment results in a three dimensional crystalline network of linked TiO 6 octahedra [20][21][22].…”
Section: Introductionmentioning
confidence: 99%
“…It was (Table 1). Hydrothermal treatment at 90 • C for 10 h is used to ensure the formation of an anatase structure before calcination [16,17]. The phase transformation from anatase to rutile does not occur in TiO 2 materials during calcination at high temperatures, so only the anatase phase is present at 600 • C, without any other crystalline by-products.…”
Section: Photocatalytic Activitymentioning
confidence: 99%
“…Titania (TiO 2 ) with wide bandgap semiconductor has recently attracted much attention because of its large surface area and pores, which are of great importance in photocatalysis, highly specific chemical sensors, luminescence, self-cleaning surfaces, carbon nanotubes and solar cells [1,2]. Notably, TiO 2 is one of the most widely used photocatalysts due to its high photocatalytic efficiency and thermostability.…”
Section: Introductionmentioning
confidence: 99%