Synthesis and characterization of Ni-doped TiN thin films deposited by jet electrodeposition

Xia, Fafeng; Jia, Wanchun; Ma, Chunyang; Yang, Rong; Wang, Y.; Potts, M.

doi:10.1016/j.apsusc.2017.10.203

Cited by 74 publications

(15 citation statements)

References 14 publications

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“…However, as the PF increased from 100 to 150 Hz, the majority of TiN nanoparticles were equally distributed, resulting in nanocomposites with uniform, dense, and fine organizations (Figure 5c). Increased PF could give more energy to adsorb the insoluble nanoparticles, as revealed by previous research findings [3,8,23]. Higher frequencies resulted in homogenous binding of a significant quantity of TiN nanoparticles with Ni 2+ and W 6+ ions in Ni-W/TiN nanocomposites, increasing the deposited TiN content in the coatings, even though the DC remained constant at varied pulse frequencies.…”

Section: Surface Morphologymentioning

confidence: 57%

“…Ceramic-particle-reinforced metal-based nanocomposites (CPRMNs) have been widely utilized in compression engines and internal combustion and in petroleum tools as well as in friction parts for many years due to their excellent properties, including excellent wear resistance, high surface hardness, good cooling performance, and corrosion resistance [1][2][3][4][5][6][7][8]. CPRMNs can be made in a variety of ways, including electrodeposition, chemical deposition, and brush plating.…”

Section: Introductionmentioning

confidence: 99%

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Influence of Duty Cycle and Pulse Frequency on Structures and Performances of Electrodeposited Ni-W/TiN Nanocomposites on Oil-Gas X52 Steels

et al. 2021

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This paper describes the pulse current electrodeposition (PCE) mediated preparation of Ni-W/TiN nanocomposites. Pulse current electrodeposition (PCE) was used to make Ni-W/TiN nanocomposites. The nanoindentation, wear, and corrosion of deposited Ni-W/TiN nanocomposites were studied using X-ray diffraction (XRD) and scanning electron microscopy (SEM). The influence of pulse frequency (PF) and duty ratio on the shape, structure, phase structure, wear, and corrosion resistance of Ni-W/TiN nanocomposites was studied. When the duty cycle (DC) was 10%, the results demonstrated that a considerable number of fine grains were present on the deposited Ni-W/TiN nanocomposites, forming smooth, uniform, and fine organization. Increasing DC decreased the content of TiN nanoparticles in Ni-W/TiN nanocomposites. The content of TiN nanoparticles reduced from 11.3 wt % to 7.3 wt % by increasing the DC from 10% to 50%. In contrast, as the PF was increased, the TiN content in Ni-W/TiN nanocomposites increased. When the PF was increased from 50 Hz to 150 Hz, the TiN content increased from 6.4 wt % to 9.6 wt %, respectively. Furthermore, with a PF of 150 Hz and a DC of 10%, the produced Ni-W/TiN nanocomposites had an average hardness of 934.3 HV with ~39.8 µm of an average thickness. The weight loss of the Ni-W/TiN nanocomposites was just 17.2 mg at a PF of 150 Hz, demonstrating the excellent wear resistance potential. Meanwhile, the greatest impedance was found in Ni-W/TiN nanocomposites made with a DC of 10% and a PF of 150 Hz, indicating the best corrosion resistance.

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Section: Surface Morphologymentioning

confidence: 57%

Section: Introductionmentioning

confidence: 99%

Influence of Duty Cycle and Pulse Frequency on Structures and Performances of Electrodeposited Ni-W/TiN Nanocomposites on Oil-Gas X52 Steels

et al. 2021

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“…Electrodeposition method is a commonly used method to get different metals (such as copper, nickel, cadmium, zinc, etc.) [1][2][3][4] and different coatings (such as alloy coatings, composite coatings) [5][6][7] . The principle is simple: a voltage is applied between the cathode and the anode to produce a current, thus forming a metallic deposit on the surface of the cathode [8,9] .…”

Section: Introductionmentioning

confidence: 99%

Simulation and Experimental Research on Nickel-based Coating Preparedby Jet Electrodeposition at Different Scanning Speeds

Xiu-qing

Zhang

et al. 2021

Preprint

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In order to study the processing mechanism of jet electrodeposition and explore the influence of different scanning speed on the wear and corrosion resistance of nickel-based coating prepared by jet electrodeposition. The reciprocating scanning motion of the nozzle was used to prepare the nickel-based coating in a specific area. Combined with COMSOL software, the coupling effect of multiple physical fields in the process of jet electrodeposition at different scanning speeds was numerically calculated. Scanning electron microscope, microhardness tester, material surface comprehensive performance tester and electrochemical workstation were used to analyze the surface morphology, section thickness, microhardness, abrasion resistance and corrosion resistance of the nickel-based coating prepared by jet electrodeposition at different scanning speeds. Results show that with the increase of scanning speed, coating grain size decreases, and the coating thickness increases after the first decreases, and microhardness increase after decreases first, abrasion resistance and corrosion resistance were lower after increase first, When the scanning speed reaches 600mm/min, the jet electrodeposited nickel-based coating has the best performance, the maximum thickness reaches 24.83μm, the microhardness reaches 616.86HV, and the wear scar area is 2766.75μm2. In addition, the self-corrosion potential is -0.33V, the self-corrosion current density is 5.16E-7A·cm2, and the equivalent impedance is 4660Ω. The experimental results are consistent with the simulation results, which verifies the accuracy of the simulation model and provides theoretical guidance for further experiments related to jet electrodeposition.

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“…Meanwhile, the agglomeration of the nanoparticles is broken up during the high-speed flushing, and the nanoparticles are distributed uniformly in the coating. Therefore, using jet electrodeposition to prepare nanoparticles reinforced composite coating, the advantages of high deposition efficiency, uniform distribution of nanoparticles and good surface quality of coating can be obtained [8][9][10].…”

Section: Introductionmentioning

confidence: 99%

Efficient Preparation of Nanoparticles Reinforced Nickel-based Composite Coating with Highly Preferred (220) Orientation

Jin

Liu

et al. 2020

Preprint

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This paper reports a phenomenon that the grain orientation gradually evolves to (220) with the deposition current density increasing when preparing nanoparticles reinforced nickel-based composite coatings by jet electrodeposition (JED). During the preparation of Ni-SiC composite coatings, the deposition current density increases from 180 A/dm2 to 220 A/dm2, and TC(220) gradually increases from 41.4% to 97.7% correspondingly.The Ni-SiC composite coating with highly preferred (220) orientation has superior corrosion resistance and adhesion force. With the increase of TC(220), the surface roughness is reduced from Ra1.210 μm to Ra0.119 μm, the self-corrosion potential increases from -0.747 V to -0.477 V, the corrosion current density decreases from 54.52 μA·cm2 to 2.76 μA·cm2, the diameter of corrosion pits that after 10 days of immersion in 3.5 wt% NaCl solution decreases from 3.3~22.2 μm to 153~260 nm, and the adhesion of the coating is increased from 20.5 N to 61.6 N.The research results can provide theoretical and technical support for the preparation of new composite coatings with high efficiency, low cost, high adhesion and strong corrosion resistance.

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Synthesis and characterization of Ni-doped TiN thin films deposited by jet electrodeposition

Cited by 74 publications

References 14 publications

Influence of Duty Cycle and Pulse Frequency on Structures and Performances of Electrodeposited Ni-W/TiN Nanocomposites on Oil-Gas X52 Steels

Influence of Duty Cycle and Pulse Frequency on Structures and Performances of Electrodeposited Ni-W/TiN Nanocomposites on Oil-Gas X52 Steels

Simulation and Experimental Research on Nickel-based Coating Preparedby Jet Electrodeposition at Different Scanning Speeds

Efficient Preparation of Nanoparticles Reinforced Nickel-based Composite Coating with Highly Preferred (220) Orientation

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