2006
DOI: 10.1007/s10593-006-0074-6
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Synthesis and extraction properties of oxathiacrown compounds containing benzyl groups

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Cited by 4 publications
(3 citation statements)
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“…After 12 h of stirring at 65 °C, the reaction was worked up and purified as described above to yield compound 4 as an oil (0.223 g, 80% yield): R f = 0.87 (hexanes/EtOAc 70:30 v/v); 1 H NMR (CDCl 3 , 500 MHz) δ 7.37–7.27 (m, 5H), 4.41–4.33 (m, 1H), 3.83 (dd, J = 10.5, 4.2 Hz, 1H), 3.64 (dd, J = 10.4, 8.9 Hz, 1H), 3.51 (dd, J = 14.5, 4.8 Hz, 1H), 3.14 (dd, J = 14.5, 7.8 Hz, 1H); 13 C NMR (CDCl 3 , 125 MHz) δ 136.9, 129.5, 128.5, 127.2, 52.4, 42.0, 36.0. 1 H and 13 C NMR spectral data are consistent with previously reported values …”
Section: Methodssupporting
confidence: 92%
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“…After 12 h of stirring at 65 °C, the reaction was worked up and purified as described above to yield compound 4 as an oil (0.223 g, 80% yield): R f = 0.87 (hexanes/EtOAc 70:30 v/v); 1 H NMR (CDCl 3 , 500 MHz) δ 7.37–7.27 (m, 5H), 4.41–4.33 (m, 1H), 3.83 (dd, J = 10.5, 4.2 Hz, 1H), 3.64 (dd, J = 10.4, 8.9 Hz, 1H), 3.51 (dd, J = 14.5, 4.8 Hz, 1H), 3.14 (dd, J = 14.5, 7.8 Hz, 1H); 13 C NMR (CDCl 3 , 125 MHz) δ 136.9, 129.5, 128.5, 127.2, 52.4, 42.0, 36.0. 1 H and 13 C NMR spectral data are consistent with previously reported values …”
Section: Methodssupporting
confidence: 92%
“…1 H and 13 C NMR spectral data are consistent with previously reported values. 25 trans-1,2-Dibromocyclohexane (8). The standard procedure was used with cyclohexene (101 μL, 1.0 mmol), HBr (48% aq, 0.56 mL, 5 mmol), and DMSO (1 mL).…”
Section: ■ Experimental Sectionmentioning
confidence: 99%
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