Synthesis and properties of palladium nanoparticles by pulsed laser ablation in liquid

Mendivil, M.I.; Krishnan, Bindu; Castillo, G. Alan; Shaji, Sadasivan

doi:10.1016/j.apsusc.2015.03.075

Cited by 28 publications

(12 citation statements)

References 17 publications

Supporting

Mentioning

Contrasting

Order By: Relevance

“…For 5 minutes of ablation at lower fluence (9 J/cm 2 ), Pt NPs obtained in all these media showed nearly the same average size (2 ± 1 nm), but there was an increase in average size with increase in fluence for all the three liquid media. Increase in energy fluence could result in increase in average size of nanoparticles as reported in many cases [12,16,19,20]. The effects of ablation time (at constant energy fluence of 25 J/cm 2 ) were different in these liquids.…”

Section: Resultsmentioning

confidence: 81%

“…We reported synthesis of metal, semiconductor, and ceramic nanoparticles using pulsed laser ablation in liquid technique in which the shape, size, structure, composition, and optical properties were analyzed [12][13][14][15][16][17][18]. In this paper, we report the effects of liquid medium (acetone, ethanol, and methanol), ablation energy fluence, and ablation time on morphology, size, structure, composition, and optical properties of platinum nanoparticles produced by PLAL technique.…”

Section: Introductionmentioning

confidence: 99%

See 1 more Smart Citation

Synthesis and Properties of Platinum Nanoparticles by Pulsed Laser Ablation in Liquid

Palma

Krishnan

Castillo-Rodríguez

et al. 2016

Journal of Nanomaterials

View full text Add to dashboard Cite

Platinum (Pt) nanoparticles were synthesized by pulsed laser ablation in liquid (PLAL) technique in different liquids (acetone, ethanol, and methanol). Ablation was performed using a Q-switched Nd:YAG laser with output energy of 230 mJ/pulse for 532 nm wavelength. Ablation time and laser energy fluence were varied for all the liquids. Effects of laser energy fluence, ablation time, and nature of the liquid were reported. The mean size, size distributions, shape, elemental composition, and optical properties of Pt nanoparticles synthesized by PLAL were examined by transmission electron microscopy (TEM), X-ray photoelectron spectroscopy (XPS), and UV-Visible absorption spectroscopy.

show abstract

Section: Resultsmentioning

confidence: 81%

Section: Introductionmentioning

confidence: 99%

Synthesis and Properties of Platinum Nanoparticles by Pulsed Laser Ablation in Liquid

Palma

Krishnan

Castillo-Rodríguez

et al. 2016

Journal of Nanomaterials

View full text Add to dashboard Cite

show abstract

“…The ultrasonic bath post treatment of LAL-produced Si NPs can reduce their (hydrodynamic) size over time, and performing this treatment in HF can help remove oxygen from the synthesized particles . As expected, ultrasonication is also effective at redispersing precipitated laser-generated NPs in solution . For biological applications, ,− ex situ and in situ bioconjugation methods allow the efficient functionalization of laser-produced charged particles with proteins, DNA, and functional ligands. ,, Ex situ conjugation is much more effective in preserving the molecular function as compared to in situ conjugation because LFL-triggered degradation does not occur during the conjugation period. , Additionally, the ex situ downstream processing method has been reported for LAL to produce similar biological targeting properties as compared to the in situ bioconjugation method …”

Section: Material Process Liquid and Laser Parametersmentioning

confidence: 89%

“…136 As expected, ultrasonication is also effective at redispersing precipitated laser-generated NPs in solution. 557 For biological applications, 363,558−560 ex situ and in situ bioconjugation methods allow the efficient functionalization of laser-produced charged particles with proteins, DNA, and functional ligands. 232,308,561 Ex situ conjugation is much more effective in preserving the molecular function as compared to in situ conjugation because LFL-triggered degradation does not occur during the conjugation period.…”

Section: Chemical Reviewsmentioning

confidence: 99%

Laser Synthesis and Processing of Colloids: Fundamentals and Applications

2017

View full text Add to dashboard Cite

Driven by functionality and purity demand for applications of inorganic nanoparticle colloids in optics, biology, and energy, their surface chemistry has become a topic of intensive research interest. Consequently, ligand-free colloids are ideal reference materials for evaluating the effects of surface adsorbates from the initial state for application-oriented nanointegration purposes. After two decades of development, laser synthesis and processing of colloids (LSPC) has emerged as a convenient and scalable technique for the synthesis of ligand-free nanomaterials in sealed environments. In addition to the high-purity surface of LSPC-generated nanoparticles, other strengths of LSPC include its high throughput, convenience for preparing alloys or series of doped nanomaterials, and its continuous operation mode, suitable for downstream processing. Unscreened surface charge of LSPC-synthesized colloids is the key to achieving colloidal stability and high affinity to biomolecules as well as support materials, thereby enabling the fabrication of bioconjugates and heterogeneous catalysts. Accurate size control of LSPC-synthesized materials ranging from quantum dots to submicrometer spheres and recent upscaling advancement toward the multiple-gram scale are helpful for extending the applicability of LSPC-synthesized nanomaterials to various fields. By discussing key reports on both the fundamentals and the applications related to laser ablation, fragmentation, and melting in liquids, this Article presents a timely and critical review of this emerging topic.

show abstract

“…Laser ablation was used to disperse Pt-NPs in acetone [27], water [28], and methanol [26]. The effect of time and the pulsed energy were the significant parameters used for the evaluation of the shape and particle size of Pt-NPs [29]. Hence, Pt-NPs are capable of forming in organic and inorganic solutions using a laser ablation method.…”

Section: Introductionmentioning

confidence: 99%

Optical and Thermal Properties of Laser-Ablated Platinum Nanoparticles Graphene Oxide Composite

Sadrolhosseini

Habibiasr

Shafie

et al. 2019

IJMS

View full text Add to dashboard Cite

Platinum nanoparticles were synthesized in graphene oxide aqueous solution using a laser ablation technique to investigate the effect of optical linear, nonlinear and thermal properties of platinum-graphene oxide nanocomposite solution. The samples were prepared with different ablation times. The platinum nanoparticles that formed a spherical shape on the surface of graphene oxide solution were authenticated using UV-visible spectrum and transmission electron microscopy patterns. The particle size decreased with increasing ablation time, and the concentration and volume fraction of samples were increased. To obtain the optical linear, nonlinear and thermal properties of platinum-graphene oxide nanocomposite solution, UV-visible spectroscopy, Z-scan, thermal lens and photoacoustic techniques were used. Consequently, the linear and nonlinear refractive indices increased with an increase in the volume fraction of platinum nanoparticles. It was observed from the spatial self-phase modulation patterns that, the optical nonlinear property of the graphene oxide was enhanced in the presence of platinum nanoparticles, and the nonlinearity increased with an increase in the volume fraction of platinum nanoparticles inside the graphene oxide solution. The thermal diffusivity and thermal effusivity of platinum nanoparticles graphene oxide were measured using a thermal lens and photoacoustic methods, respectively. The thermal diffusivity and thermal effusivity of samples were in the range of 0.0341 × 10−5 m2/s to 0.1223 × 10−5 m2/s and 0.163 W s1/2 cm−2 K−1 to 0.3192 W s1/2 cm−2 K−1, respectively. Consequently, the platinum enhanced the optical and thermal properties of graphene oxide.

show abstract

Synthesis and properties of palladium nanoparticles by pulsed laser ablation in liquid

Cited by 28 publications

References 17 publications

Synthesis and Properties of Platinum Nanoparticles by Pulsed Laser Ablation in Liquid

Synthesis and Properties of Platinum Nanoparticles by Pulsed Laser Ablation in Liquid

Laser Synthesis and Processing of Colloids: Fundamentals and Applications

Optical and Thermal Properties of Laser-Ablated Platinum Nanoparticles Graphene Oxide Composite

Contact Info

Product

Resources

About