Synthesis and Spectral Studies of Some New bis(1,3‐Diketonato)palladium(II) Complexes

Pathak, Vijai N.; Oza, Chandra K.; Tiwari, Ranjana; Chaudhary, Sarita

doi:10.1081/sim-120020327

Cited by 4 publications

(3 citation statements)

References 32 publications

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“…: 137-138ºC, Lit m.p. : 111-113ºC (Pathak et al, 2003). 1 H-NMR (CDCl3) δ 7.87 (d, 2H, J=8.5 Hz, Ar-H), 7.75 (d, 1H, J=15.6 Hz, =CH), 7.62 (d, 2H, J=8.5 Hz, Ar-H),7.35 (d, 1H, J=15.5 Hz, =CH), 7.16 (s, 1H, Ar-H), 7.12 (dd, 1H, J=8.0 Hz, 1.6 Hz, Ar-H), 6.85 (d, 1H, J=8.0 Hz, Ar-H), 6.03 (s, 2H, -OCH2O-).…”

Section: (E)-3-(benzo[d][13]dioxol-5-yl)-1-(4bromophenyl)prop-2-en-1-one (Pc6)mentioning

confidence: 99%

Design, Synthesis and Biological Activities of Chalcones with Piperonal Moiety

Tuğrak

Gül

Anil

et al. 2020

Erzincan Üniversitesi Fen Bilimleri Enstitüsü Dergisi

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Heterocyclic compounds are of specific significance between pharmacologically active compounds. In this study, some piperonal-based chalcones (PC1-PC10) were synthesized with Claisen-Schmidt Condensation with the reaction between 3,4-methylenedioxybenzaldehyde and several acetophenones. Inhibition potency of the chalcones were evaluated toward human carbonic anhydrase I and II enzymes (hCA I and hCA II), and acetylcholinesterase (AChE). The chalcone derivatives were found to have IC50 values in the range of 5.11-109.70 μM for hCA I, 17.05-162.59 μM for hCA II, and 18.52-98.69 μM for AChE. All compounds showed lower inhibition potential than reference compounds. While the PC3 (methoxy derivative) compound was the most effective compound against both hCA I and hCA II, PC5 (fluorine derivative) showed the strongest inhibition effect against AChE in the series. Results confirmed that the chalcone derivatives PC3 and PC5 can be considered as favorable candidates against hCA I, hCA II and AChE isoenzymes to design more potent enzyme inhibitors.

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Section: (E)-3-(benzo[d][13]dioxol-5-yl)-1-(4bromophenyl)prop-2-en-1-one (Pc6)mentioning

confidence: 99%

Design, Synthesis and Biological Activities of Chalcones with Piperonal Moiety

Tuğrak

Gül

Anil

et al. 2020

Erzincan Üniversitesi Fen Bilimleri Enstitüsü Dergisi

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“…In terms of the CVD experiments in this work, the main subjective was to investigate the deposition performance of these compounds depending on the nature of the reactive gases, oxygen and forming gas (N 2 /H 2 , 90/10, v/v). 27,28 with Haccp (synthesis of 7) or Hacch (synthesis of 8) in the molar ratio of 1 : 4 in methanol at ambient temperature in presence of sodium carbonate (Scheme 1, Experimental section). Aer appropriate workup, 7 and 8 could be isolated as yellow solids in a yield of 80% (7) or virtually quantitative yield (8) (Experimental section).…”

Section: Introductionmentioning

confidence: 99%

Bis(β-diketonato)- and allyl-(β-diketonato)-palladium(ii) complexes: synthesis, characterization and MOCVD application

et al. 2016

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“…Furthermore, -diketones have attracted attention due to their distinct structural properties and high synthetic utility [15][16][17][18][19][20]. Metal complexes containing -diketonato bidentate ligands have been reported as photosensitizers [21], magneto-optical materials [22], insulin mimetic chelates [23] and antitumor compounds [24].…”

Section: Introductionmentioning

confidence: 99%

Trichloro-mono- β -diketonato oxorhenium(V) complexes: synthesis, characterization and crystal structure

Das

Sarkar

Patra

et al. 2008

Journal of Coordination Chemistry

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Oxorhenium(V) complexes of -diketonate systems have been synthesized and isolated in pure form. The red complexes n-Bu 4 N[ReO(R 1 COCHCOR 2 )Cl 3 ] (acac, R 1 ¼R 2 ¼CH 3 ; bzac, R 1 ¼CH 3 and R 2 ¼C 6 H 5 ; bzbz, R 1 ¼R 2 ¼C 6 H 5 ) have been characterized by elemental analyses, spectroscopic and other physico-chemical tools. One complex, n-Bu 4 N[ReO(bzbz)Cl 3 ] (1c) has been subjected to single-crystal X-ray analysis. In the structure of the anion, the metal has a six-coordinate octahedral environment in which the bidentate -diketone ligand is cis and trans to the terminal oxygen.

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Synthesis and Spectral Studies of Some New bis(1,3‐Diketonato)palladium(II) Complexes

Cited by 4 publications

References 32 publications

Design, Synthesis and Biological Activities of Chalcones with Piperonal Moiety

Design, Synthesis and Biological Activities of Chalcones with Piperonal Moiety

Bis(β-diketonato)- and allyl-(β-diketonato)-palladium(ii) complexes: synthesis, characterization and MOCVD application

Trichloro-mono- β -diketonato oxorhenium(V) complexes: synthesis, characterization and crystal structure

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