Synthesis, Characterization, and Applications of Metal Nanoparticles

Shnoudeh, Abeer Jabra; Hamad, Islam; Abdo, Ruwaida W.; Qadumii, Lana; Jaber, Abdulmutallab Yousef; Surchi, Hiba Salim; Alkelany, Shahd Z.

doi:10.1016/b978-0-12-814427-5.00015-9

Cited by 223 publications

(144 citation statements)

References 487 publications

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“…The reason for the decrease in IFT at this concentration can be attributed to the increase in conductivity the presence of active ions (charge effect) in the environment [ 70 ]. To prove this effect, according to Figure 11 which shows the conductivity of the prepared nanofluids, one can see that conductivity of the nanofluids increases linearly with an increasie in concentration [ 71 , 72 ]. However, at concentration of 500 ppm, the graph shows an anomalous behavior where conductivity increases (increased net charge effect of the ions and the related electrical double-layer interactions in the environment) at this concentration [ 73 , 74 , 75 , 76 ].…”

Section: Resultsmentioning

confidence: 99%

Synthesis, Characterization, and Assessment of a CeO2@Nanoclay Nanocomposite for Enhanced Oil Recovery

et al. 2020

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In this paper, synthesis and characterization of a novel CeO2/nanoclay nanocomposite (NC) and its effects on IFT reduction and wettability alteration is reported in the literature for the first time. The NC was characterized using scanning electron microscopy (SEM), X-ray diffraction (XRD), Fourier-transform infrared spectroscopy (FTIR), thermogravimetric analysis (TGA), energy-dispersive X-ray spectroscopy (EDS), and EDS MAP. The surface morphology, crystalline phases, and functional groups of the novel NC were investigated. Nanofluids with different concentrations of 100, 250, 500, 1000, 1500, and 2000 ppm were prepared and used as dispersants in porous media. The stability, pH, conductivity, IFT, and wettability alternation characteristics of the prepared nanofluids were examined to find out the optimum concentration for the selected carbonate and sandstone reservoir rocks. Conductivity and zeta potential measurements showed that a nanofluid with concentration of 500 ppm can reduce the IFT from 35 mN/m to 17 mN/m (48.5% reduction) and alter the contact angle of the tested carbonate and sandstone reservoir rock samples from 139° to 53° (38% improvement in wettability alteration) and 123° to 90° (27% improvement in wettability alteration), respectively. A cubic fluorite structure was identified for CeO2 using the standard XRD data. FESEM revealed that the surface morphology of the NC has a layer sheet morphology of CeO2/SiO2 nanocomposite and the particle sizes are approximately 20 to 26 nm. TGA analysis results shows that the novel NC has a high stability at 90 °C which is a typical upper bound temperature in petroleum reservoirs. Zeta potential peaks at concentration of 500 ppm which is a sign of stabilty of the nanofluid. The results of this study can be used in design of optimum yet effective EOR schemes for both carbobate and sandstone petroleum reservoirs.

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Section: Resultsmentioning

confidence: 99%

Synthesis, Characterization, and Assessment of a CeO2@Nanoclay Nanocomposite for Enhanced Oil Recovery

et al. 2020

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“…The ZP value is a very important parameter for the evaluation of the stability of nanoparticle suspensions (Honary and Zahir, 2013 ). When nanoparticles are stabilized with low molecular weight surfactants, mainly through electrostatic interactions, it is considered that ZP values higher than 25 mV point to very good stability (Shnoudeh et al, 2019 ). However, when stabilization is achieved with high molecular weight stabilizers (steric stabilization) ZP values of only 20 mV or lower can provide sufficient repulsive forces and good stabilization (Honary and Zahir, 2013 ).…”

Section: Resultsmentioning

confidence: 99%

Comparative Study of the Antimicrobial Activity of Selenium Nanoparticles With Different Surface Chemistry and Structure

Filipović

Ušjak

Milenković

et al. 2021

Front. Bioeng. Biotechnol.

141

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Although selenium nanoparticles (SeNPs) have gained attention in the scientific community mostly through investigation of their anticancer activity, a great potential of this nanomaterial was recognized recently regarding its antimicrobial activity. The particle form, size, and surface chemistry have been recognized as crucial parameters determining the interaction of nanomaterials with biological entities. Furthermore, considering a narrow boundary between beneficial and toxic effects for selenium per se, it is clear that investigations of biomedical applications of SeNPs are very demanding and must be done with great precautions. The goal of this work is to evaluate the effects of SeNPs surface chemistry and structure on antimicrobial activity against several common bacterial strains, including Staphylococcus aureus (ATCC 6538), Enterococcus faecalis (ATCC 29212), Bacillus subtilis (ATCC 6633), and Kocuria rhizophila (ATCC 9341), as well as Escherichia coli (ATCC 8739), Salmonella Abony (NCTC 6017), Klebsiella pneumoniae (NCIMB 9111) and Pseudomonas aeruginosa (ATCC 9027), and the standard yeast strain Candida albicans (ATCC 10231). Three types of SeNPs were synthesized by chemical reduction approach using different stabilizers and reducing agents: (i) bovine serum albumin (BSA) + ascorbic acid, (ii) chitosan + ascorbic acid, and (iii) with glucose. A thorough physicochemical characterization of the obtained SeNPs was performed to determine the effects of varying synthesis parameters on their morphology, size, structure, and surface chemistry. All SeNPs were amorphous, with spherical morphology and size in the range 70–300 nm. However, the SeNPs obtained under different synthesis conditions, i.e. by using different stabilizers as well as reducing agents, exhibited different antimicrobial activity as well as cytotoxicity which are crucial for their applications. In this paper, the antimicrobial screening of the selected systems is presented, which was determined by the broth microdilution method, and inhibitory influence on the production of monomicrobial and dual-species biofilm was evaluated. The potential mechanism of action of different systems is proposed. Additionally, the cytotoxicity of SeNPs was examined on the MRC-5 cell line, in the same concentration interval as for antimicrobial testing. It was shown that formulation SeNPs-BSA expressed a significantly lower cytotoxic effect than the other two formulations.

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“…The magnitude of zeta potential gives a prediction of the colloidal stability. Zeta potential of nanoparticles with absolute values greater than 25 mV have a high degree of stability [ 57 ]. Pumpkin polysaccharides were negatively charged on the interface, with zeta potential values ranging from −26.5 to −33.0 mV ( Figure 3 B), suggesting good emulsifying properties [ 58 ].…”

Section: Resultsmentioning

confidence: 99%

Physicochemical Properties and Antioxidant Activity of Pumpkin Polysaccharide (Cucurbita moschata Duchesne ex Poiret) Modified by Subcritical Water

Zhao

Wei

et al. 2021

Foods

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In this paper, subcritical water (SCW) was applied to modify pumpkin (Cucurbita moschata Duchesne ex Poiret) polysaccharides, and the properties and antioxidant activity of pumpkin polysaccharides were investigated. SCW treatments at varying temperature led to changes in the rheological and emulsifying properties of pumpkin polysaccharides. SCW treatments efficiently degraded pumpkin polysaccharides and changed the molecular weight distribution. Decreases in intrinsic viscosity, viscosity-average molecular weight, and apparent viscosity were also observed, while the activation energy and flow behavior indices increased. The temperature of SCW treatment has a great influence on the linear viscoelastic properties and antioxidant activity of pumpkin polysaccharides. Pumpkin polysaccharides solution treated by SCW at 150 °C exhibited the highest emulsifying activity and antioxidant activity, which was probably due to a broader molecular mass distribution and more reducing ends exposed after treatment. Scanning electron microscopy showed that SCW treatment changed the microstructure of pumpkin polysaccharides, resulting in the exposure of bigger surface area. Our results suggest that SCW treatment is an effective approach to modify pumpkin polysaccharides to achieve improved solution properties and antioxidant activity.

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Synthesis, Characterization, and Applications of Metal Nanoparticles

Cited by 223 publications

References 487 publications

Synthesis, Characterization, and Assessment of a CeO2@Nanoclay Nanocomposite for Enhanced Oil Recovery

Synthesis, Characterization, and Assessment of a CeO2@Nanoclay Nanocomposite for Enhanced Oil Recovery

Comparative Study of the Antimicrobial Activity of Selenium Nanoparticles With Different Surface Chemistry and Structure

Physicochemical Properties and Antioxidant Activity of Pumpkin Polysaccharide (Cucurbita moschata Duchesne ex Poiret) Modified by Subcritical Water

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