Synthesis, characterization and polymerization of novel sugars based on methacrylate

Koruyucu, Meryem; Saltan, Fehmi; Kök, Gökhan; Akat, Hakan; Salman, Yeşim

doi:10.1007/s13726-016-0437-5

Cited by 4 publications

(2 citation statements)

References 19 publications

Supporting

Mentioning

Contrasting

Order By: Relevance

Section: Synthesis Crystallization and Spectroscopic Detailsmentioning

confidence: 99%

“…Topiramate azidosulfate was synthesized using a modification of procedures found in the literature (Maryanoff et al, 1987;Kankan et al, 2004;Arvai et al, 2006;Koruyucu et al, 2016). The synthesis involved three steps, viz., (1) synthesis of 2,3:4,5 bis-O-(1-methylethylidene)--d-fructopyranose, (2) synthesis of 2,3:4,5-bis-O-(1-methylethylidene)-1-chlorosulfate--dfructopyranose, and (3) synthesis of topiramate azidosulfate (I), as depicted in Fig.…”

Section: Synthesis Crystallization and Spectroscopic Detailsmentioning

confidence: 99%

See 1 more Smart Citation

Synthesis and crystal structure of topiramate azidosulfate at 90 K and 298 K

Priyanka¹,

Jayanna²,

Kumar

et al. 2022

Acta Cryst E

View full text Add to dashboard Cite

The low (90 K) and room (298 K) temperature crystal structures of topiramate azidosulfate [systematic name 2,3:4,5-bis-O-(1-methylethylidene)-β-D-fructopyranose azidosulfate], C12H19N3O8S, an intermediate in the synthesis of the anti-convulsant drug topiramate, are described. Topiramate azidosulfate (I) finds use as a reference impurity standard for topiramate. A modified synthesis and some spectroscopic details are also presented.

show abstract

Section: Synthesis Crystallization and Spectroscopic Detailsmentioning

confidence: 99%

Section: Synthesis Crystallization and Spectroscopic Detailsmentioning

confidence: 99%